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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004345
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C : \HPCHEM\ 1 \DATA\DEC2 70130708.D Vial: 49 Acq On : 30 Dec 2001 6:21 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 2-Propanone, 1-(1-methylethoxy Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

18.16 0.27 ug/1 168085 Acenaphthene-dl0 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1-(1-methylethoxy) - 116 C6H1202 042781-12-4 23 2 Guanidine, /methyl- 73 C2H7N3 000471-29-4 9 3 Hydroperoxide, 1-ethylpropyl 104 C5H12O2 024254-57-7 9 4 2-Hexanone, 5-methyl- 114 C7H14O 000110-12-3 9 Abundance- T ~ Scan 1428 (18.156 min): 30708.D(-) m/ z 43.00 100.00% 43

57 73 5000 111 95 10390025 । rrl ■ 7 । । rr| । n i 11 17.80 18.00 18.20 18.40 myonsypanajimm +p4—#+r8P h 127 TTTTTPWWINPI] 146 m/z->.... 10 20 30 40 50 60 70 80 90 100110 120130140 150 160 170 180190 200 201 'i " " i m/ z 57.0.0 60.70% Abundance #3286: 2-Propanone, 1-(1-methylethoxy)- 43 5000 TTTT T Ifrrt 1"T ID 17.80 18.00 18.20 18.40 27 11 58 73 m/z 73.00 52.43% _ _____ 11, " I ■ ■' ‘ 11' ‘ * I' i. I. 1................. . | I ’’ I’ ’’ I ■ ' ' ' | ' ' ' ■ | ' ' ' '| ' ' ‘ ■ | ' ' > ' | ■ ' ' ' | ' ■ ' ' | ' ' ‘ ' | ‘ ' | ।'"|,,, , | , II I| IIII|II I!| II I!| m/z-> 10 20 30 40 50 60 70 80 90 100110120130140 150 160170 180190 200 Abundance 452524: Guanidine, methyl- 30 43 73 “PRetTT I 17.80 18.00 18.20 18.40 5000 m/z 111.10 42.83% 57 17 i 1I—T, TTTTTTTTTDWTVTTTNTWTTTTTTTTTTTTTTTTTRTTTTPTTTTTTTTTTTT m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 - Abundance #1916: Hydroperoxide, 1-ethylpropyl 43 17.80 18.00 18.20 18.40 57 m/ z 69.0.0 24.62% 71 5000 27

86 104 ‘'i"" i" "l1'"I ""i1" r'1' i' ■" i" " i ■'" r "' r1 ‘' r "' i" " i —PTPTMT m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 17.80 18.00 18.20 18.40

30708.D GCMS1126.M Mon Jan 28 11:28:41 2002 Page 6

NYC-WTC_000004345

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NYC-WTC_000004345Source: NYC Law Department, mirrored locally

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