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GCMS analysis results for sample AD29563, Jan 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036712–000036728

Folder label: “GCMS X 12/7/01 A 1/2/02”

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Scanned page image, NYC-WTC_000036725
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\29563.D Vial: 36 Acq On : 28 Dec 2001 11:11 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C: \DATABASE\NBS75K. L

Peak Number 7 N-(Trifluoroacetyl)-0,O011-t Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.79. 1.10 ug/1 583903 Phenanthrene-dl0 24.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N- (Trifluoroacetyl) -O, O’, O ‘‘-tris (t 481 C19H34F3NO4Si3 000000-00-0 43 2 N-(Trifluoracetyl)-0,0 ,0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 43 3 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 4 N-(Trifluoroacetyl)N,0,0 ‘,0‘‘-tetr 553 C22H42F3NO4Si4 000000-00-0 27 Abundance in 1933 (22.787 min): 29563.D (-) m/z 73.0.0 100.00%] 73

5000 147 355

m/z--> 45 — TTPAT 50 117 100 150 191 TIT’ — 200 251 I 250 300 327 :350 221

400 281

450 4 500 550 22.40 22.60 22.80 23.00 23.20 m/z 147.00 25.90% Abundance #58326: N-(Trifluoroacetyl)-O,O',O"-tris(trimethylsilyl)no 73

355 ----- . ...... — 5000- 22.40 22.60 22.80 23.00 23.20 m/z 355.05 22.32% 45 । 120147 193 265 481 • > । ■ miz-> 50 100 150 200 250 300 350 400 450 500 550 'Abundance #58807: N-(Trif)uoracetyi)-O,O'.O"-tns(trimethylsilyljepin 73 -------............. , 355 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.05 17.44%

45 ■i 140 184 281 j 480 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] ■ i ■ ■ ■ • i ■ ---- ------- , 73 355 22.40 22.60 22.80 23.00 23.20 m/z 281.00 13.53% 5000-

1........ 45 — 208 251 281 386 458 548 ................. ------ 22.40 22.60 22.80 23.00 23.2G m/z—> 50 100 150 200 250 300 350 400 450 500 550

29563.D GCMS1126.M Tue Jan 08 11:42:34 2002 Page 7

NYC-WTC_000036725

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NYC-WTC_000036725Source: NYC Law Department, mirrored locally

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