GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
NYC-WTC_000036712–000036728Folder label: “GCMS X 12/7/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\29563.D Vial: 36 Acq On : 28 Dec 2001 11:11 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C: \DATABASE\NBS75K. L
Peak Number 7 N-(Trifluoroacetyl)-0,O011-t Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
22.79. 1.10 ug/1 583903 Phenanthrene-dl0 24.98
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 N- (Trifluoroacetyl) -O, O’, O ‘‘-tris (t 481 C19H34F3NO4Si3 000000-00-0 43 2 N-(Trifluoracetyl)-0,0 ,0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 43 3 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 4 N-(Trifluoroacetyl)N,0,0 ‘,0‘‘-tetr 553 C22H42F3NO4Si4 000000-00-0 27 Abundance in 1933 (22.787 min): 29563.D (-) m/z 73.0.0 100.00%] 73
5000 147 355
m/z--> 45 — TTPAT 50 117 100 150 191 TIT’ — 200 251 I 250 300 327 :350 221
400 281
450 4 500 550 22.40 22.60 22.80 23.00 23.20 m/z 147.00 25.90% Abundance #58326: N-(Trifluoroacetyl)-O,O',O"-tris(trimethylsilyl)no 73
355 ----- . ...... — 5000- 22.40 22.60 22.80 23.00 23.20 m/z 355.05 22.32% 45 । 120147 193 265 481 • > । ■ miz-> 50 100 150 200 250 300 350 400 450 500 550 'Abundance #58807: N-(Trif)uoracetyi)-O,O'.O"-tns(trimethylsilyljepin 73 -------............. , 355 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.05 17.44%
45 ■i 140 184 281 j 480 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] ■ i ■ ■ ■ • i ■ ---- ------- , 73 355 22.40 22.60 22.80 23.00 23.20 m/z 281.00 13.53% 5000-
1........ 45 — 208 251 281 386 458 548 ................. ------ 22.40 22.60 22.80 23.00 23.2G m/z—> 50 100 150 200 250 300 350 400 450 500 550
29563.D GCMS1126.M Tue Jan 08 11:42:34 2002 Page 7
NYC-WTC_000036725
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NYC-WTC_000036798
GCMS analysis report for sample AD29523 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034180
Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034988
Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004149
Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017675
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30251 conducted on January 9, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018546
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017782
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD303B5 conducted on January 10, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000036689
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
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NYC-WTC_000036690
Laboratory results for GCMS blank analysis of sample AD29522 showing detection levels below method detection limits.
Filed in the same folder
NYC-WTC_000036695
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
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NYC-WTC_000036703
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000036704
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder