DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30709.D Vial: 47 Acq On : 30 Dec 2001 4:24 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 11 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

31.71 1.73 ug/1 764444 Chrysene-dl2 33.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 2 2-Hexenedioic acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 23 3 Ethanedioic a.cp.&, bis (trimethylsily 234 C8H1804Si2 018294-04-7 23 4 1,1,1,5,7,7,7/Heptamethyl-3,3-bis(t 444 C13H4005Si6 _ 038147-00-1 17 Abundance Scan 2905 (31.713 min): 30709.D (-) m/z 73.00 1 00.00% 73

5000- 147 221 261 2EE 45 0- ■ ■ ‘I ' r 117 ’ , 191, 249, .. 327, L., 401 42% 31.40 31.60 31.80 32.00 m/z 147.00 40.86% m/z-> 50 100 150 200 250 300 _ 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 147 .. y... 31.40 31.60 31.80 32.00

221 m/z 221.05 23.37% I 281i 327 t 415.............. 519 561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #40777: 2-Hexenedroic acid. ns(trimethylsily!) ester (E)- 73

31.40 31.60 31.80 32.00 5000- m/z 281.0.0 15.63% 147 45 244 273 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #30580: Ethanedioic acid, bis(trimethylsilyl) ester ‘I TTIII 73 147 31.40 31.60 31.80 32.00 m/z 355.05 10.60% 5000 45

, J 11^ ....................... . , . . . ....... . , . I ■ ■ ■ 1 I m/z—> 50 100 150 200 250 300 350 400 450 500 550 31.40 31.60 31.80 32.00

30709.D GCMS1126.M Mon Jan 28 11:33:27 2002 Page 11

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