GCMS analysis report, sample AE04419, April 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2102\4419.D Vial: 10 Acq On : 21 Mar 2002 8:09 pm Operator: Sample : gc/ms scan 3/1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

38.85 0.49 ug/1 58309 Perylene-dl2 37.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H520 i7 071579-69-6 23 2 Benzeneethanamine, N- [ (pentafluorop 563 C24H34F O3S13 055429-13-5 9 3 1,2-Benzenedicarboxylic acid, bis(t 310 C14H22q4Si2 002078-22-0 9 4 N-Meth adrenaline, tri-TMS 413 C19H39NO3Si 000000-00-0 9 Abundance 73 Scan 3683 (38.855 min): 4419.D (-) ym/z 73.00 1 00.00%

147 5000 221 355 281 , 253 |l 429 38.60 38.80 39'00 39.20 :miz-> +49. 50 100 193 1 3274— — - *1***I4***I* 150 200 250 300 350 400 450 500 550 m/z 147.00 62.68% (Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-trls(trim 73

5000 A) ,MAA M/,, MM M

•? 147 38.60 38.80 39.00 39.20 m/z 221.05 45.60% 221 281 327 415 519 561 ■ 1 r m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #7470e Benzeneethanamine, N-ipentaflccrophenyh)methylene] 73 355 38.60 38.80 39.00 39.20 5000 m/z 355.05 31.18%

miz-> Abundance

5000 45 208 251 281 50 100 150 200 250 300 350 400 450 500 550 73 386

#72973:1,2-Benzenedicarboxylic acid, bis(trimethylsilyl) e 147 458 548

T 1 ‘ I** 38.60 38.80 39.00 39.20 m/z 281.00 24.16%

45 295

, .1,. .1'.., 193271 .. ■ ■ i 1 ‘ 1 ' i ‘ 1 1 ■ i • • ■ ■ i 1 ‘ ■ i ■ 1 ■ ■ i ' ' miz-> 50 100 150 200 250 300 350 400 450 500 550 38.60 38.80 39.00 39.20

4419.D GCMS0308.M Fri Mar 22 09:42:03 2002 Page 4

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