GCMS analysis results for sample AE05897, March 29 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR2102\5897,D Vial: 25 Acq On : 22 Mar 2002 12:56 pm Operator: Sample : gc/ms scan 3/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

40.64 0.45 ug/T 81713 Perylene-dl2 37.99 / Hit# of 5 itative ID MW MolForm CAS# Qual

1 3-Isopropoxy 1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 25 2 Noradrenal ini tetra-TMS 457 C20H43NO3Si4 000000-00-0 10 3 1,2-Benzensdicarboxylic acid, bis(t 310 C14H22O4Si2 002078-22-0 9 4 Benzoic ac/id ,5-bis(trimethylsilo 370 C16H30O4Si3 .003618-20-0 9 Abundance *" Scan 3877 (40.640 min): 5897.D (-) m/ Z 73

147 5000 221

281 44 [ I 227| ] 429 40.40 40.60 40.80 41.00 + m/z 146.95 60.37%

IC ____ 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1.1,1,7,7,7-hexamethyl-3,5,5-tris(irim 73

\A/^/vV [III 5000 147 40.40 40.60 40.80 41.00__ m/z 221.05 49.63% I m/2->50 Abundance

5000 I, I I

73 100

102 150 200__ 250 281

300 327

:350 400 J-57Se' 7 \o!ttdi-e>ialins teVa-iMS

355 415 450 519 500 561 550

40,40 40.60 40.80 41.00 m/z 355. Q.5 1.. 31.60%

45 147 I !m/z-> w50 100... 150 200 250 300 350 400 442 450 500 550 Abundance #72972: 1.2-Benzenedicarboxyiic acid, bis(trimethylsilyl) e ‘M-rn-rr-r-r-r 147 4040 40.60 40.80 41.00__ m/z -281.0.0 ' 24.5^ 73 5000

45 295 I I 'm/2-> 50 100 150 200 250 300 350 400 450 500 550 40.40 40.60 40.80 41.00

5897.D GCMSOSOS.M Mon Mar 25 14:27:30 2002 Page 4

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