GCMS analysis results for sample AE04388, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR2502\4388.D Vial: 15 Acq On : 26 Mar 2002 12:01 am Operator: Sample : gc/ms scan 2/28 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-1sopropoxy-1,1,1,7,7,7-hexam Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

37.38 0.70 ug/1 52713 Perylene-dl2 37.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy/l, 1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 25 2 Trisiloxane/ 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 16 3 1,2-Benzenedicarboxylic acid, bis (t 310 C14H2204Si2 002078-22-0 9 4 Benzoic acid. 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 9 Abundance Scan 3522 (37.376 min): 4388.D (-) 73 147 5000 221 281 355 . 429 37.00 37.20 37.40 37.60 37.80 44 Tr 193 253 I I 327, ...000 m/z 147.00 64.16% m/z-> 50 166 150 266 250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyi-3,5,5-tts(trim 73

5000 AA-—AAA-—AMAAAAA 147 37'00 37.20 37.40 37.60 37.80 221 281 327 m/z 221.05 42.81% 415 519 561 1 m/z->. 50 100 '156 ‘ 200 250 300 350 400 ' 450 500 550 . Abundance 5159 " irtand 1 ■ :ms5moamoadB/sstmo- 73 147 1 I ' ‘ ‘ ' I 1 1 1 1 | h rj * ■ 1 * 281 37.00 37.20 37.40 37.60 37.80 5000 m/z 281.10 30.60% 369 207 249 338 miz-> 50 IPO 150 200 250 300 350 400 450 500 550 Abundance #72972:1,2-Benzenedicarboxylic acid, bis(trimethylsilyl) e 147 37.00 37.20 37.40 37.60 37.80 73 m/z 355.05 29.63% 5000

45 295 ——— — 119 —— 193221 ■ I . ’ I ‘ ‘ I ‘ ‘ TI8 ‘ 14 I ‘ miz-2. 50 100 150 200 250 300 350 400 450 500 550 37.00 37.20 37.40 37,60 37.80

4388.D GCMS0308.M Thu Mar 28 12:31:14 2002 Page 3

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