GCMS analysis results for sample AE04035, Mar 2002

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Data File : C:\HPCHEM\1\DATA\MAR2202\4035.D Vial: 41 Acq On 24 Mar 2002 9:33 am Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

37.39 1.03 ug/1 94277 Perylene-dl2 37.97

Hit# of 5 / Tentative ID MW MolForm CAS# Qual

1 3-Isoprop6xy-l,1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 37 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 22 3 1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 20 4 1,2-Benzenedicarboxylic acid, bis(t 310 C14H2204Si2 002078-22-0 14 Abundance Scan 3524 (37.393 min): 4035.D (-) m/z 73.0.0 100.00% 73 \ 147 I 5000 221 281 355 I/ __ 429 1 37.00 37.20 37.40 37.60 37.80 49 Tt 1 TT I 1 1 193 ■I ' ' 11" ,1 1 2531 113271. I 1 ' ■ i 1 1 ' 1 । 1 1 401 , ' ' i 1 1 ' 1 i ' - | m/z 147.00 59.14% m/z-> 50 100 150 200 250 300 350 400 450 500 550 ... _ Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 147 ' 37.00 37.20 37.40 37.60 37.80

221 281 i m/ Z 221.05 46.70% 327 J____ L ,L 415 519 561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance 73 147 1 ' i ' ' 37.00 37.20 37.40 37.60 37.80 5000 m/z 355.05 30.55% 281 45 369 —........ 117 , 207 249............................................................... m/z-> 50 .. 100__ 150__ 200 250. 300.. 350 400 450 500 550 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether .. I hk i ■ ■ ■ ■ i ■ 1 ■ ■ । 73 37.00 37.20 37.40 37.60 37.80 m/z 281.05 2 6.49% 207 5000 147 34 103 281

m/z-> ' ' I ' ' ' ' I ' ' 50 100 1 J'1 TT I I 150 200 1 I I 1 I 250 300 350 325 400 -2 450 500 550 37.00 37.20 37.40 37.60 37.80

4035.D GCMS0308.M Tue Mar 26 10:48:23 2002 Page 3

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