GCMS analysis results for sample AE04035, Mar 2002

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Data File : C:\HPCHEM\1\DATA\MAR2202\4035.D Vial: 41 Acq On : 24 Mar 2002 9:33 am Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Monolinoleoylglycerol trimet Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

36.15 0.43 ug/1 39098 Perylene-d12 37.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 42 2 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 23 3 Ethanedioic/acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 10 4 Amodiaquine 355 C20H22C1N3O 000086-42-0 9 Abundance 73 Scan 3389 (36.154 min): 4035.D (-) ! m/z 73.0,0 100.00%

147 5000 221 281 355 429 35.80 36.00 36.20 36.40 ---------------Hr , 253, | , —— ........ — , 191 I 1 ' 1 1 1 1 1 1 1 327 ■ [m/z 147.00 50.94% m/z-? 50 100 150 200 250 300 350 400 450 500 550 ( Abundance #58871: 1-Monolinoieoylglycerol trimethylsilyl ether

73 207 A 5000 147 1 I 11 1 1 1 1 ' 4' 1 —.......... A 35.80 36.00 36.20 36.40 34 103 281 m/z 221.05 37.00% i • ' 1 I ■ 1 I ----- ......... — 325........, 482 ........ — miz—>__ —. 50 100 150 200 250 300 350 400 450__ 500 550 Abundance 1'1 oetmalBmmgg . 73

35.80 36.00 36.20 36.40 5000 m/ z 355.05 23.08% 147

221 281 327 415 519 561 m/z-> 50....... 100 150 200 So 300 350 400 450 500 550 Abundance #71006: Ethanedioic acid, bis(trimethylsilyl) ester 73 35.80 36.00 36.20 36.40

5000-

m/z—> 45

' 1 1 11 50 117 100 147

, 150 190 219 ————— 200 250 300 350 400 450 500 550 "T AwAww WWWw ‘I 35.80 36.00 36.20 36.40 TT

4035.D GCMS0308.M Tue Mar 26 10:48:19 2002 Page 2

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