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GCMS analysis results for sample AD303B5, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD303B5 conducted on January 10, 2002.

NYC-WTC_000017782–000017795

Folder label: “GCMS X 12/13/01 A 12/27/01

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Scanned page image, NYC-WTC_000017794
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30355.D Vial: 7 Acq On : 27 Dec 2001 5:59 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Benzeneethanamine, N-[(pentafl Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.78 0.51 ug/1 167134 Phenanthrene-dl0 24.98

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43 2 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 38 3 N-(Trifluoroacetyl)-0,0’,O’’-tris(t 481 C19H34F3NO4Si3 000000-00-0 37 4 Cyclopentasiloxane, decamethyl- 370 C10H30Q5Si5 000541-02-6 25 Abundance Scan 1932 (22.785 min): 30355.D (-) m/z 73.00 100.00% 73

5000 147 - 1 | i r ■ ■ | ■ i Yi jN-T mPm" । i 1 221 281 355 22.40 22.60 22.80 23.00 23.20 ; 45 117 191, I 249 I 3 ?7 [ 401 - —fan I**.G*m/I**T*1G*I* m/z 147.10 26.11% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-((pentafluorophenyl)methylene] 73 355

5000 22.40 22.60 22.80 23.00 23.20 m/z 355.0 21.04% 45 ‘ J 1 208 251 281 386 458 548 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #73975: Benzoic acid, 2,4-bis(trimethylsilyl)oxy]-. trimet 73

22.40 22.60 22.80 23.00 23.20 5000 355 m/z 221.05 17.15% 45 , _______ 133 193 223 281______________________ m/z-> 50 100 ' 150 ' ' 200 250 300 350 400 450 500 550 ........ ).......... Abundance #58326: N-(Trifluoroacetyl)-O,O',O’'-tris(trimethylsilyl)no 73 2240 22.60 22*80 23.00 23.20 355 m/z 281.00 14.59% 5000

45 — 120147 193 265 481 T1dddm////d///0//mmnmmr 1 < ' I 1 1 1 1 I ' ' m/z-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20

30355.D GCMS1126.M Wed Jan 02 10:55:55 2002 Page 6

NYC-WTC_000017794

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NYC-WTC_000017794Source: NYC Law Department, mirrored locally

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