GCMS analysis results for sample AD30352, Jan 2002

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Data File : C:\HPCHEM\l\DATA\DEC2701\30352.D Vial: 19 Acq On : 28 Dec 2001 5:38 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C: \DATABASE\NBS75K . L ********************************************************************* Peak Number 9 Benzeneethanamine, N-[(pentafl Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

22.79 2.88 ug/1 1331530 Phenanthrene-dl0 24.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 37 3 N-(Trifluoroacetyl)-0,0',O’'-tris(t 481 C19H34F3NO4Si3 000000-00-0 37 4 N-(Trifluoracetyl)-0,0’,O»-tris(tri 495 C20H36F3NO4Si3 000000-00-0 37 Abundance Scan 1933 (22.787 min): 30352.D (-) m/z 72.95 100.00% 73

5000 147 . 355 I | i i i । । t । । । । 1 । » t । j »“ r "i" j1 r } 221 281 I 1 45 1 , 117 191, [ 249, | 327 [ 401 441 22.40 22.60 22.80 23.00 23.20 rhinaan ■ "—*Tn ‘ fT —— rm--rT13T **I4*I"11 l"‘ ‘ m/z 147.0,0 26.52% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-K(pentafluoropheny!)methylene] 73 355 %

5000 22.40 22.60 22.80 23.00 23*20 45 m/z 355.0 24.80% i 208 251.281 _ 386 458 548 i 1 1 *i * ■ 1 ■ i 1 ■ TIK—g.mmBOTT “ ‘ • I ‘ J ‘ ‘ I* ‘ ‘ ‘ 141* * m/z-> 50 100 150 200 250 300350400450500550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 22.40 22.60 22.80 23.00 23.20 267 5000 m/z 221.0,5 17.24%

207 323 1 ' i 11 *I***I*I***I***1*1*1* "* । । > । i 11 i miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58326: N-(Trffluoroacetyl)-O,O'.O”-Ms(trimethylsilyl)no 73 22.40 22.60 22.80 23.00 23.20 355 m/z 281.00 14.05% 5000

45 120147 193 265 481 7 « j ) 1‘ i j i i i > J i j i s 1t UI f"* j i r 1 i JT i T' i j I i i । 1 i r j J 1 i i I gT miz—> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 '23.00 23.20

30352.D GCMS1126.M Wed Jan 02 10:50:50 2002 Page 9

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