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GCMS analysis log for sample AD31024

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31024 performed on January 18, 2002.

NYC-WTC_000017494–000017513

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017508
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NYC 9/11 Public Portal Document Library Search Compound Report _ °°" pata File : C:\HPCHEM\1\DATA\JAN0802\31024.D Vial: 16 Acq On : 9 dan 2002 3:58 am Operator: 209 GALOS Sample : goms scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L eve Vererrrrr rrr enter ererrerrrtrrrrtrrrrrrlitrrtt itr t ttt ttt rit rirt ry Peak Number 8 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 8 R.T. EstCone Area Relative to ISTD Re? 26.73 0.76 ug/l 254034 Phenanthrene-d10 24.80 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 33 2 Mandelic acid ditbdms 380 C20H3603Si2 078324-07-9 25 3 Ethanedioic acid, bis(trimethylsily 234 CeH1804si2 018294-04-7 25 4 _3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H52078i7 __071579-69-6 23 oundarcs 7 ‘Scan 2362 (26.731 miny: 31024.D (-) ae m/z 73.00 100.00 5000} | | | 147 ] 224 281 7 45 355 az9 | 26402660 26.80 27:00 96 117 191 249 327 401 429 m/z 147.00 33.63 mmlz>___40._60._80_ 100 120 140 160 180 200 220 240 260 260 300 320 340 360 380400420 | \ Abundance #52459: Tisloxane, 1,1,1,5.5.5hexamethyl3,3-bis|(vimet | | B 147 | i 26.40 26.60 26.80 27.00 369 m/z 281.0, 16.00 at 249 338. : : eereerepere mz 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420. | ‘Abundarice f \ 73 1a7 26.40 26.60 _26.80_ 27.00 a 224 nes m/z 221.0) 13.84% 323 47 118 189 287 . z->__ 40, 60. 80 100 120 140 160 180 200 230 240 260 280 300 320 340 360 380 400 420 Abundance #30680: Ethanedioic acid, bis(trimethyisily)) ester wn 147, 26.40 26.60 26.80 27.00 m/z 74.00 8.98 5000: | 145 1|, 190 219 | I | riz» "40 60 80 100 120 140 160 180 200 200 240 260 280 300 320 340 360 380 400420 | 2640.26.60 26.80 27100. | 31024.D GCMS0103.M Wed Jan 09 12:15:17 2002 Page 8 \ NYC-WTC_000017508

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NYC-WTC_000017508Source: NYC Law Department, mirrored locally

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Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31020 on January 18, 2002.

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Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996

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GCMS scan comments for sample AD30605 · Box DEP Box 16

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GCMS analysis log for sample AD31076 · Box DEP Box 16

NYC-WTC_000017514

Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31076 on January 18, 2002.

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GCMS blank analysis results · Box DEP Box 16

NYC-WTC_000017344

Laboratory report listing detection limits for numerous organic compounds in a GCMS blank sample analyzed on January 10, 2002.

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