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GCMS analysis log for sample AD31020

Machine-extracted title · confidence 95%

Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31020 on January 18, 2002.

NYC-WTC_000017459–000017477

Folder label: “GCMS X 12/20/01 A 1/8/02”

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Scanned page image, NYC-WTC_000017474
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NYC 9/11 Public Portal Document g . Library Search Compound Report “+ Data File : C:\HPCHEM\1\DATA\JANO802\31020.D Vial: 15 ‘ Acq On : 9 Jan 2002 2:59 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L eTeerrcrrrrrrrrer re srrerrererrrerrrrr rrr tir rr tr trrettrt irri tert rosy Peak Number 9 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 9 R.T. EstCone Area Relative to ISTD R.T. 26.73 0.55 ug/L 171296 Phenanthrene-d10 24.81 Hit# of 5 Tentative ID MW MolForm CASH Qual 1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 42 2 Ethanedioic acid, bis(trimethylsily 234 CeH1so4si2 018294-04-7 32 3 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 _4 2-Hexenedioic acid, bis(trimethylsi 288 C12H2404Si2 _055494-10-5 23 Abundance —————S*S*~S*S*~S*«San 28S (26.73 minh: 1020.0) Taz 73 “90 100.00 | i | 5000 ; PP og 355 ‘26140 261602680 27.00 14! i 428 00 28.80.27. BL oh Ht | 242 |, Efe 147.00 32-228 mis> 80 100.450 _ 200.250 300350400 450__500 550 i) ‘Abundance ee ‘Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis{(trimet i ‘5000 7 | ae 60 sea ea 360 m/z 281.00 16.30% a | miz-> 50100. 150-200-250 300 350400450500. 550_ \ | ‘Abundance 7 3 147 26.40 26.60 26.80 27.00 5000 m/z 221.0, 14.61 45 190 a9 miz>___ 80100160 200 250 300 a0 400 490 500 650 Abundance ‘#60503: 3-isopropoxy-1,1,1,7,7,7-hexamethyt-3,5,5-tris(trim 26.40 26.60 _26.80_27.00 m/z 74.00 9.83 | a sar 48 519 561_| i miz—> 90100 180 200 250 300 360 400 450 500 550 | 26.40 2660 2660 2700 | 31020.D GCMS0103.M Wed Jan 09 12:11:59 2002 Page 9 NYC-WTC_000017474

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NYC-WTC_000017474Source: NYC Law Department, mirrored locally

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