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GCMS analysis log for sample AD31020

Machine-extracted title · confidence 95%

Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31020 on January 18, 2002.

NYC-WTC_000017459–000017477

Folder label: “GCMS X 12/20/01 A 1/8/02”

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Scanned page image, NYC-WTC_000017475
OCR text

OCR status: ocr · source: ours

NYC 9/11 Public Portal Document . Library Search Compound Report “* Data File : C:\HPCHEM\1\DATA\JAN0802\31020.D Vial: 15 L Acq On : 9 Jan 2002 2:59 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ee verererrrrr rarer rere rerrrrrrrrerrrrrrrrrrttrttritt ttt rtttt ttt tri ty Peak Number 10 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 11 R.T. EstCone Area Relative to ISTD R.T. 30.09 0.47 ug/l 96523 Chrysene-d12 32.84 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 38 2 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H4005Sié6 038147-00-1 28 3 N-Methyladrenaline, tri-TMS 413 C19H39NO3Si3 000000-00-0 12 4 Silanamine, N-[2,6-dimethyl-4-[(tri 281 C14H27NOSi2 _072088-09-6 9 Roundanca ~~ Sean 2726 (80.004 min 31020.0 ©) m/z aa 100.008 15000. } 147 | 2 og, ass error 429 29.80 30.00 30.20 30.40. Bee Madre t Mle ab Bele OM tee | Be LAT OG 33 15 miz~>___ 50.100 150 200 250 300 350 __ 400450 _500_550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethy!-3,5,5-tris(trim t | hid ain ie so Se m/z 221.0) 20.60% art Lie 519561 mz-> 50-100 150-200-250 300 350 400-450-500 550. Abundance i 3 147 |"2e/60" 30.00 30.20 30.40 | 5000 267 m/z 281.00 12.278 355 ae | h i 207 | | mi» "80. 100180200 250 900 350400450600 560 | Abundance ‘#54808: N-Methyladrenaline, t-TMS CO eeeegpoeebepereopeo 7B 29.80 30.00 30.20 30.40 | | m/z 355.0) 11.29%) ‘5000: 365, | | | 45 a 267 309 mz-> 80100180 200. 250 300 380 400480 600580. | 20160 30.00 30.20 3040. | 31020.D GCMS0103.M Wed Jan 09 12:12:04 2002 Page 10 NYC-WTC_000017475

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NYC-WTC_000017475Source: NYC Law Department, mirrored locally

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