NYC 9/11 Public Portal Document
. Library Search Compound Report
: ‘Data File : C:\HPCHEM\1\DATA\JAN0802\30605.D Vial: 17
Acq On : 9 dan 2002 4:56 am Operator: 209 GALOS
Sample : gems scan 12/20 Inst : GC/MS 209
Mise : Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
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Peak Number 14 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 10
R.T. EstCone Area Relative to ISTD R.T.
32.93 0.93 ug/1 189788 Chrysene-d12 32.84 i
Hit# of 5 Tentative ID MW MolForm cas# Qual
1 Trisiloxane, A,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 38
2 1,1,1,3,5,5/7,7,7-Nonamethyl-3- (tri 384 C12H3604Si5 038146-99-5 22
3 3-Isoprop9ky-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 12
4 Ethanedigic acid, bis(trimethylsily 234 CsH1804si2 018294-04-7 12
(Abundance ‘Scan 3038 (32.931 min): 30605.D (-) m/z 73.00 100.00%
i
|
j ‘5000: 147
| | = 28" 355
7
: 429 32.60 32.80 33.00 33.20
' oe rs ae eee Ao m/z 147.00 49.41%
fz ___ 50 100 150 200 250 300 350 400 450 500 550
frBundance 6 #74103: Trisiloxane, 1,1,1,5,5,S-hexamethyl-3,3-bis[(trimet
i | 147 |
! |
io 2a s2le0 ‘32100 ‘sa.00 3520" |
i 5 200 m/z 221.00 27.85
ki 417, 207 249 |
mz 50. 100 _150 200 250 300 350 400 450 500 550
Pane BOE TINSEL Hanttoe sere aio
| T
281 32.60 32180 33.00 33.20
000 | 147 m/z 355.0) 18.27
|
| .
ml 207 i o
Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethy!-3,5,6-tris(trim
J 32.60_32.80_33.00_33.20
m/z 281.00 16.53
hae 147
| 281
Lh at 3, 418 510561
mz-> 50 100 150 200250 _300__350__400 _450__500__§50_| 32.60 32.80 33.00 33.20 _
30605.D GCMS0103.M Tue Jan 15 09:31:57 2002 Page 14
NYC-WTC_000017285
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