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GCMS analysis log for sample AD31073

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

NYC-WTC_000017434–000017458

Folder label: “GCMS X 12/20/01 A 1/8/02”

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Scanned page image, NYC-WTC_000017455
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NYC 9/11 Public Portal Document oe Library Search Compound Report -, * ‘Data File : C:\HPCHEM\1\DATA\JAN0802\31073.D Vial: 10 Acq On : 8 Jan 2002 10:07 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ew wwrerrrrrrrrer ret srtrrrrrrrrerrtrrrtrrttrrttttt ttt tri tritici ry Peak Number 14 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 34.22 0.71 ug/l 154362 Chrysene-d12 32.84 Hit# of 5 Tentative ID MW MolForm cAS# Qual 1 Trisiloxaxe, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 43 2 3-(3-Hy@foxyphenyl) -3-hydroxypropio 398 C18H3404Si3 000000-00-0 37 3 Propapéic acid, 2-oxo-3-(trimethyls 232 C9H2003Si2 055887-51-9 25 4 3-Isépropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7__071579-69-6 25 Abundance, ‘Scan 3178 (34.223 min): 31073.0 -) m/z 73-00 100.00% | 5000. 17 \ 24 \ | 281 358 T 429 | 33.80 34.00 34.20 34,40 34.60 “ 88,1 peter Seah arteries Aprechrr| m/z 147.00 50.40 mlz->___40_60_80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380400420 _ ‘Abundance g_ PTA: Tslxane, 1.11.8. ohexamey 3. met \ | aca oa 33180 34100 34.20 440 _ 34.60 1 as | 308 m/z 221.05 31.42 { i a7 207249 mz 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360380400420 _| | Abundarics | ] 7 267 | ] 33.80 34.00 34.20 34,40 34.60 | 0001 147 m/z 281.00 21.23% | 47 203341 | nvz-> "40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 300 380 400 420 | Abundance #30222: Propanolc acid, 2-oxo-3-(trimethylsilyl}, timethy i 147 33.80 34.00 34.20 34.40 34.60 { ? m/z 355.05 17.48! 5000: 45 27 47 180 leer miz-> "40. 60. 80 100 120 140 160 180 260 220 240 260 280 300 320 340 360 380 400 420" | 33/80 34.00 34.20 3440 34.60 31073.D GCMS0103.M Wed Jan 09 12:19:56 2002 Page 14 NYC-WTC_000017455 ‘

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NYC-WTC_000017455Source: NYC Law Department, mirrored locally

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