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GCMS analysis log for sample AD31073

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

NYC-WTC_000017434–000017458

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017454
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NYC 9/11 Public Portal Document fe Library Search Compound Report “'. + "Data File : C:\HPCHEM\1\DATA\JAN0802\31073.D Vial: 10 Acq On : 8 Jan 2002 10:07 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESSE ISI ISIS SII O GI IO GEI IEEE IOSIII TI IIE IOI IIIS III II III II IIIA Peak Number 13 1-Monolinoleoylglycerol trimet Concentration Rank 11 R.T. EstCone Area Relative to ISTD R.T. 32.93 1.24 ug/1 270222 Chrysene-d12 32.84 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 1-Monolinoleg¥lglycerol trimethylsi 498 C27H5404Si2 054284-45-6 45 2 Ethanedioip”acid, bis(trimethylsily 234 caH1s04si2 018294-04-7 32 3 2-Hexenegfoic acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 23 4 Butanoi¢’ acid, 3-methyl-2-[(trimeth 262 C11H2603Si2 __055124-92-0 23 Abundance - ‘Scan 3037 (32.929 min): 31073.0 ¢) | m/z 73.00 100.00 | ‘5000: 147 | 24 281 355 oT 7 429 | “seleo “sz!e0 ‘33.00. 33.20 | BB ah My heh bE ue m/z 147.00 42.95% mz> 50. 100150200250 3008504004 { ‘Abundance #88871: 1-Monolinolecyigiycerol trimethylsilyl ether | | 207 | 147 i Saari | 18000; i |. 32.60_32.80_33,00 . 33.20 * 103 | | | 281 [m/z 221.00 24.17% | 305 i | mz-> ‘so 100150200250 30088040048 | ‘Abundance ij 1 | 73 i 17 | “galeo “az'e0 ‘39.00 38.20 5000 m/z 281.00 15.46% 45 | i 117 190 219 | ‘Abundancs WOTTT. 2Hexenedioic acid, bis(timethyisily) ester, (E> . 32.60 _32.80_33.00_33.20 { m/z ore 13.33% 5000 | i és 147 | | 412 2a4 273 | miz-> ‘50. 100 150. -200~=—« 250-300 380 400.450 | “szleo’ ‘32180. 33100 3320. | 31073.D GCMS0103.M Wed Jan 09 12:19:52 2002 Page 13 NYC-WTC_000017454

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NYC-WTC_000017454Source: NYC Law Department, mirrored locally

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