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GCMS analysis log for sample AD31073

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

NYC-WTC_000017434–000017458

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017453
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NYC 9/11 Public Portal Document la Library Search Compound Report . ° ‘Data File : C:\HPCHEM\1\DATA\JAN0802\31073.D Vial: 10 Acq On : 8 Jan 2002 10:07 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\i\METHODS\GCMS0103.M (RTE Integrator) Title + 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESS IIIS ISI IGE EI EIS OI ISS ISS IIS I IIIS CIO TOI TIS IOI IIE 5 Peak Number 12 2-Hexenedioic acid, bis(trimet Concentration Rank 12 R.T. EstCone Area Relative to ISTD R.T. 31.56 1.05 ug/l 228297 Chrysene-di2 32.84 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 2-Hexenedioig“acid, bis(trimethylsi 288 C12H2404si2 055494-10-5 23 2 Butanoic a, 3-methyl-2-[(trimeth 262 C11H2603Si2 055124-92-0 23 3 Ethanediefc acid, bis(trimethylsily 234 CaHiso4si2 018294-04-7 23 4 3-Isopyopoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 17 Rbundance ‘Sean 2688 (81.561 min}: 310730 () 7 pm/z 73-90 = 5000- 147 | 221 Pl ~ ~ | 355, 429 31.20 31.40 31.60 31.80 AS At? — 194 7 251 he 327 ‘ 401 m/z 147.00 21.52 mmiz~>____40_60_80_ 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400.420 | | ‘Abundance T #40777: 2-Hexenedioic acid, bis(trimethyisilyl) ester, (E)- | ea? 147 — 31203140. L. “80. | . | m/z 221.0) 24.87% Li 12 244 273 . | nntz->_ "a 60” 80 100 120 140 160 180 20220 240 280 280 300 320 340 300 860 400 420 | Abundances Be van 9G imedheisiiilea. 1 | | 13 | | us . | | i 31.20 3140 31.60 3180 | | 5000} i m/z 281.00 15.54 a7 190 219 247 | mmiz>__ 40.60. 80 100 120 140 160 180 200 220 240 260 280 300 320 340 960 300 400 420 | \ Abundance #80580: Ethanedioic acd, bis(timethyisiy) ester 147 31.20 31.40 31.60 31.80 _- m/z 355.05 11.70 : 45 | | | 180 a6 | miz-> 40 60.80 100 120 140 160 180 200 220 240 260 280 300 320 340 360380400420 | 31.20. 31.40. 31.60. 31.80 31073.D GCMS0103.M Wed Jan 09 12:19:47 2002 Page 12 NYC-WTC_000017453 ,

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NYC-WTC_000017453Source: NYC Law Department, mirrored locally

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