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GCMS analysis log for sample AD31073

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

NYC-WTC_000017434–000017458

Folder label: “GCMS X 12/20/01 A 1/8/02”

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Scanned page image, NYC-WTC_000017452
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OCR status: ocr · source: ours

NYC 9/11 Public Portal Document a, Library Search Compound Report “. + “Data File : C:\HPCHEM\1\DATA\JAN0802\31073.D Vial: 10 Acq On : 8 dan 2002 10:07 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst. : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P . Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L eerenrrrrrrrrsererrsrererrnrrerrrrrtrrrrrrrtrr ttt rrr trtiti iret i rr try Peak Number 11 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 9 R.T. EstCone Area Relative to ISTD R. Ts 30.09 1.30 ug/l 283371 Chrysene-di2 32.84 Hit# of 5 Teneative ID MW MolForm CAS# Qual 1 1,1,1,5,7,7/7-Heptamethyl-3,3-bis(t 444 C13H#4005Si6 038147-00-1 28 2 Benzoic agfd, 2,4-bis[(trimethylsil 370 C16H30048i3 010586-16-0 12 3 3-Trimet}Hylsilyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 12 4 Silananfine, N-[2,6-dimethyl-4-[(tri 281 C14H27NOSi2 __072088-09-6 12 Rouridancs ‘Scan 2728 (80.082 miny: 31073. () “m/z 73.00 100.008 | 5000: 147 a 281 365 429 29,80 30.00 30.20 30.40 Pega Ml 7 fe PE rchemmipmrinn| m/z 147.00 35.37 rmiz—>_ "40 6080 100 120 140 160 180 200 220 240 260 20 300 320 240 360 380 400.420. | | ‘Abundance #56714: 1,1,1,5,7,7,7-Heptamethyi-3,3-bis(trimethyisiloxy)t | 73 | | ‘5 207 m/z 221.05 20.64% vz->___ "40" 60. 80 100 120 140 180 100 200 220 240 280 260 900 820 340 380 380 400 420 | Abundance - | a ae aaa | ‘5000 355 m/z 281.00 12.55 45 133 493 223 281 nnyz~>_____40_60_80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380.400 420, Abundance '#56734: 3-Trimethyillyioxystearic ac, trimethyisily est ww 29.80 30.00 30.20 30.40 m/z 355.0) 12.09 e000, 147 233 | 313 429 | 189 xo | miz-> 40. 60.80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400. ‘29180 30.00 30.20. 30.40 31073.D GCMS0103.M Wed Jan 09 12:19:42 2002 Page 11 NYC-WTC_000017452

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