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GCMS analysis log for sample AD31073

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

NYC-WTC_000017434–000017458

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017451
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OCR status: ocr · source: ours

NYC 9/11 Public Portal Document ~ library Search Compound Report “+ “Data File : C:\HPCHEM\1\DATA\JAN0802\31073.D Vial: 10 Acq On : 8 Jan 2002 10:07 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peereetrerrrerrcrer tere rerrrrrrrrrtrtrtrrtirrirrrt rrr r rir iii rit irri Peak Number 10 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 13 Eom EstConc Area Relative to ISTD R.T. 28.49) 0.97 ug/1 334391 Phenanthrene-d10 24.80 Hit# sid 5 Tentative ID MW MolForm cas# Qual 1 1,1,1,5,7,% 7-Heptamethyl-3,3-bis(t 444 C13H4005Si6 038147-00-1 36 2 1-Mgnoljrfoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 34 3 3-Isopfopoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 28 _4 BengOic acid, 2,4-bis[(trimethylsil 370 C16H30048i3 010586-16-0 25 ‘Abundano? ~~ Stan 2554 (28.495 min): 31073.0 ¢) m/z 73 Of 200004 | | | 5000: | | | 147 | {| Rt ogy 55 1 [45 497, 191 251 327, 401429 28:20_2840 2880 28.00 nes" 30 hn “i68” 300.20" Soo ka /* *47-90 34-058 AAbundanca | * HET T.A,1,8,7,7,7-Hopiametiye3, 3 bisteimethivisiion yt | | i i $0004 aid 355 azo 28.20 28.40 28.80 | | [es 207 : m/z 221.05 19.12 | ' i \ miz--> 50 100 150 200 250 300 360 400 450 500 550 Abundance, 73 | ane 28.20 2640 28.60 2860 | 5000 | 17 m/z “T 16.26% | 34 103 281 395 482 miz-> 50 100150200250 300-350 450500 850 J Abundance #60603: Slsopropoxy-1,1,1,7,7,7-hexamelhy-3.5 Stis(tim areca (28.20 28.40 28.60 28.80. m/z 281.0, 13.27% | =. 447 | | 1 miz-> 50 100 150 200 250 300 360 400 450 500 550 28.20 28.40 28.60 28.80 31073.D GCMS0103.M Wed Jan 09 12:19:38 2002 Page 10 1 NYC-WTC_000017451

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NYC-WTC_000017451Source: NYC Law Department, mirrored locally

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