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GCMS scan comments for sample AD30605

Machine-extracted title · confidence 95%

Laboratory note stating that the GCMS scan of sample AD30605 did not reveal unusual compounds on January 22, 2002.

NYC-WTC_000017265–000017289

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01”

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Scanned page image, NYC-WTC_000017282
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NYC 9/11 Public Portal Document . Library Search Compound Report 5 Data File : C:\HPCHEM\1\DATA\JAN0802\30605.D Vial: 17 Acq On : 9 Jan 2002 4:56 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L. eeewrerrrrr rere: SS eter rrrrrrrrrrrtrt irr ttt trtt tir trt tt ttt rit et ry Peak Number 11 1-Monolinoleoylglycerol trimet Concentration Rank 13 R.T. EstCone Area Relative to ISTD R.T. 28.50 0.76 ug/l / 257285 Phenanthrene-d10 24.81 Hit# of 5 Tepfttative ID MW MolForm cas# Qual 1 1-MonolinoJéoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 40 2 Benzoic afid, 2,4-bis[(trimethylsil 370 C16H3004Si3 010586-16-0 37 3 Benzenegthanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 35 qt 3-Isopyopoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 33 ‘Abundance ‘Scan 2555 (28.497 min): 30605.D (-) m/z 73.00 100.00 = 147 224 281 (355 28.20 28.40 28.60 28.80 __ i 45 M7, 191 249. 325, 401 429 m/z 147.00 34.69 miz->___ 50100150200 250 300 350 400 450500650 i #58871: 1-Monolinoleoyiglycerol timethyisliyl ether ! 207 : 147 1 saad 28.20 28.40 28.60 28.80 4 103 284 m/z 221.0, 18.96! i bi 482 | bz 50 100 150 200 250 300 350 400 450 500 550 nal ~ ‘#73975; Benzoic acid, 2.4-bis|(trimethyisilyl}oxy]-. trimet | ‘28.20 28.40 28160 28.80 | 000: 365 m/z 355.0 16.90) 45 i 133 493 223-284 eeeeperer rt fnlz—> 50. 100 __150_ 200 250 300 350 400 450 500 550 ‘Abundancs ~~ #74708: Berzenesthanamine, N-(pentafuorophenyiimethyiene] weep eee ! 1 "28.20_28:40 28.60 28180 i m/z 484-38 14.95 i 5000. | 4s | ' 298 251,261 306458 548, ma->__60__100_150 _200__250 300 360 _400__460_600_ 580 28.20 28.40 28.60_28.80 30605.D GCMS0103.M Tue Jan 15 09:31:43 2002 Page 11 NYC-WTC_000017282 7 —

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