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GCMS scan comments for sample AD30605

Machine-extracted title · confidence 95%

Laboratory note stating that the GCMS scan of sample AD30605 did not reveal unusual compounds on January 22, 2002.

NYC-WTC_000017265–000017289

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017283
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NYC 9/11 Public Portal Document Library Search Compound Report . Data File : C:\HPCHEM\1\DATA\JAN0802\30605.D Vial: 17 Acq On : 9 Jan 2002 4:56 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L eereetrrrrrrr reser sertrerrrrrerrrertrrrrrrrrt rrr tt rrr tri re titre tree? Peak Number 12 1-Monolinoleoylglycerol trimet Concentration Rank 8 R.T. | EstCone Area Relative to ISTD R.T. 30,09 1.11 ug/; 225938 Chrysene-d12 32.84 Hit# of 5 ‘entative ID MW MolForm cas# Qual 1 1-Monolif#foleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 28 2 1,1,1,%7,7,7-Heptamethyl-3,3-bis(t 444 C13H4005Si6 038147-00-1 25 3 TrisiYoxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 12 4 3-Isépropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 10 ‘Roundance ‘Sean 2729 (80.055 miny: 30605. () m/z 73.00 100.00 | : A at 355 | ‘ 429 29.80 30.00 30.20 30.40 45, | 95 117 soy | 251 327, 401 ae 147-00 35574 miz> 50100150200 280300850400. 450 ‘Abundance #88871: 1-Monolinoleoyigiycerol timethyisiiyi ether 207 \ 147 7 j a ] | 29,80 30.00 30.20 30.40 [ 4 | 103 7 281 m/z 221.05 19.89 i | 38, 492 > sO 150200250 350__400_-450 | indance: ‘#58714: 1.1.1.5,7,7,7-Hoptamethyl-3.3-bis(trimethylsiloxyit 3 | | 147 29.80 30.00 30.20 3040 _ | 5000. 267 m/z 355.0, 12.97 355 429 45 ar, ' ' | | 2 fz—> 50 100 150. 200 250 300 350 400 450 (Abundance #52459: Trislloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis{(trimet | 147 29.80 30.00 30.20 30.40 | oa Z 281.00 12.73 i 5000: I 369 207 o4p miz—> 50 100150200250 300380400450 29.80 30.00 30.20 30.40 30605.D GCMS0103.M Tue Jan 15 09:31:48 2002 Page 12 NYC-WTC_000017283

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NYC-WTC_000017283Source: NYC Law Department, mirrored locally

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