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GCMS scan comments for sample AD30605

Machine-extracted title · confidence 95%

Laboratory note stating that the GCMS scan of sample AD30605 did not reveal unusual compounds on January 22, 2002.

NYC-WTC_000017265–000017289

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017284
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NYC 9/11 Public Portal Document Library Search Compound Report . ‘Data File : C:\HPCHEM\1\DATA\JAN0802\30605.D Vial: 17 Acq On : 9 Jan 2002 4:56 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESSIE SII IO EEO SOIT IIS ISSO TOSI TOTTI TIT IIIS TITS I III A Peak Number 13 2-Hexenedioic acid, bis(trimet Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 31.56 0.86 ug/l 175256 Chrysene-d12 32.84 Hit# of 5 entative ID MW MolForm caAS# Qual 1 2-HexenedjSic acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 23 2 2-Ethyl-7-trimethylsilyloxy(trimeth 276 C12H2803S8i2 000000-00-0 23 3 Ethanedfoic acid, bis(trimethylsily 234 C8H1804si2 018294-04-7 16 4 Pentandic acid, 2-[(trimethylsilyl) 262 C11H26038i2 055887-46-2 12 SXbundance ‘Scan 2889 (31.563 min}: 30605.D (-) m/z 73.00 100.00: i | S000 147 | 221 281 36 429 |_31.20 31.40 31.60 31.80 | 45 417 an 249 xr, 401 Weta ae Be mz 40_60_80 100 120 140 160 18 | 220 240 260 280 300 320 340 360 380 400 420. ‘Abundance 8 ‘#40777; 2-Hexenedicic acid, bis(trimethyisilyl) ester, (E)- | 000: | i { 147 31.20 31.40 31.60 31.80 | 45 m/z 221.0, 21.95 ate ee ou a Imiz->___ 40 60_80 100120 140 160 180 200 220: ‘920 340 360 380 400 420 (Abundance. W561 3 2-Ethy!-3-rimethyisilylony(iimethylsilyDbutyrate: i 73 | vs 31.20 31.40 31.60 31.80 | | 8000: Pn | m/z 281.00 15.11 | ' | | 4s i | 1 | 191 232 261 Sa ET ne eT ey eal hniz->___"40 6080 100 120 140 160 180 200 220: 280 300 320 340 360 380 400 420 (Abundance #71008: Ethanedioic acid, bis(timethyisilyl) ester aeeyted ep | 31.20 31.40 _31.60_31.80 | ‘ui m/z 355.0, 11.34 5000: | 45 | | { 117 190 219 Inz> 40 “G0. 80100 150 140 180 180 200 220 240 260 280 300 320 340 360 380 400 420 31.20 31.40 31.60 31.80 30605.D GCMS0103.M Tue Jan 15 09:31:52 2002 Page 13 NYC-WTC_000017284

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NYC-WTC_000017284Source: NYC Law Department, mirrored locally

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