NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 23 pages
GC/MS analysis results for sample AD30909, Jan 28 2002
Machine-extracted title · confidence 100%Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
NYC-WTC_000018693–000018715Folder label: “GCMS X 12/19/01 A 1/2/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30909.D Vial: 52 Acq On 2 Jan 2002 4:19 pm Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 2-Hexenedioic acid, bis(trimet Concentration Rank 9
R.T. EstConc Area Relative to ISTD R.T.
31.72 1.50 ug/1 306586 Chrysene-dl2 33.03
Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexenedioic acid, bis(trimethylsi 288 C12H24O4Si2 055494-10-5 23 2 Butanoic acid; 3-methyl-2-[(trimeth 262 CllH26O3Si2 055124-92-0 23 3 Ethanedioic acid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 23 4 Silanamine, N- [2,6-dimethyl-4-[ (tri 281 C14H27NOS12 072088-09-6 9 Abundance Scan 2905 (31,716 mln): 30909.D (-) m/z 73.00 100.00% 73
5000 147 221 Irrim—i ITT 1 < ■ । • • • । 281 327 _ 355 401 429 31.40 31.60 31.80 32.00 l im/z-> , 45 nmmmg ...1.... 191 117 Tn-rm- 4.2494TTM 40 60 80 100120140160180200220240260280300320340360380400420 m/z 147.00 39.36% Abundance #40777:2-Hexenedioic acid, bis(trimethylsily!) ester, (E)- 73
5000 ■ > I 1 • > » I 147 31.40 31.60 31.80 32.00 45 m/z 221.05 22.71% [ |... 112... ......... 244 ............. .............. mz-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400420 ‘ ‘ Abundance #71782; Butanoic acid. 3-methyl-2-[(trimethylsilyl)oxy]-, t 73 145 TT-p-r-r-r-r 31.40 31.60 31.80 32.00 5000 m/z 281." 14.89%
45 j | 117 190 219 247 TIITNTTTTTT TTT"Eumammmmmmm910900011 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #30580: Ethanedioic acid, bis(trimethylsily!) ester ‘ ‘ I ‘ ‘ ‘ I ‘ ‘ ‘ ‘ I ‘ ‘ ' I ‘ ‘ • I 73 147 31.40 31.60 31.80 32.00 m/z 355.05 10.35% 5000 45 190 2^9 ............................................ Tpp ‘ ’ I ’ ‘ ‘ ’ I ‘ “ • J i q I • • I | • « » I | « I • • | « I • • » r J »• ' I | I i H I. . I . | I I I I | I I I I 11 J I ! | I m/z—> 40 60 80 100120140160180200220240260280300320340360380400420 31.40 31.60 31.80 32.00TT
30909.D GCMS1126.M Fri Jan 25 11:40:50 2002 Page 12
NYC-WTC_000018711
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