Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30650.D Vial: 46 Acq On : 30 Dec 2001 3:26 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 2-Hexenedioic acid, bis(trimet Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T.
31.71 1.26 ug/1 514395 Chrysene-dl2 33.03
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Hexenedioicacid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 23 2 Butanoic acid, 3-methyl-2-[(trimeth 262 CllH26O3Si2 055124-92-0 23 3 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 23 4 1,1,1, ,7,7, 7-Heptamethyl-3,3-bis(t 444 C13H4005Si6 _ 038147-00-1 23 Abundance Scan 2905 (31.715 min): 30650.D (-) m/ z 73.00 100.00% 73
5000 147 221 281 2re 31.40 31.60 31.80 32.00 45 191 1 <. ।249 nnmmmmMpgr . 96 117 L 327L 383401 429 . । >. । n. । p ।111< । fi 11 j»T j > <. > ।. >. rf.. n । > h . 11 m/z 147.00 40.69% miz-> 40 60 80 100120140 160 180 200 220 240260280300320340360 380 400420 [Abundance #40777: 2-Hexenedioic acid, bis(trimethylsilyij ester, (E)- 73
5000 147 31.40 31.60 31.80 32.00 45 m/z 221.05 22.42% 112 | 244 273 111111 TTTT i1' "r "' r'" r ‘" i" " r ■" i" " i TCn.—mu—nDTu m/z—> 40 60 80 100 120140160180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #71782 Butanoic acid. 3-methyl2-(trimethyisilyaxl- t 73 145 31.40 31.60 31.80 32.00 5000 m/z 281.00 14.27% 45 117 . 190 219 247 m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #30580: Ethanedioic acid, bis(trimethylsilyl) ester 73 147 31.40 31.60 31.80 32.00 m/z 355.05 10.64% 5000 45 190 219 TIWmmmaupmummmuegag m/z- 40 60 80 100120140160180200220 240260 280 300 320340360380400420 31.40 31.60 31.80 32.00
30650.D GCMS1126.M Mon Jan 28 11:18:52 2002 Page 12
NYC-WTC_000004382
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
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