Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
NYC-WTC_000018470–000018491Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\30645.D Vial: 53 Acq On : 30 Dec 2001 10:14 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 11
R.T. EstConc Area Relative to ISTD R.T.
34.37 1.31 ug/1 477409 Chrysene-dl2 33.03
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy^l,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 2 Ethanedioic acid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 32. 3 Butanoi acid, 3-methyl-2-[(trimeth 262 CllH2603Si2 055124-92-0 23 4 9,12,15-Octadecatrienoic acid, 2,3- 496 C27H5204Si2 055521-22-7 23 Abundance Scan 3194 (34.367 min): 30645.D (-) m/z 73.00 100.00% 73
5000 147 221 TTI । 1 i । । 11 । t i ■ 281 355 ‘ i • * 1 . 327. 1 401 419 34.00 34.20 34.40 34.60 m/z-> 0- 451 rl • T* 50 117 , 100 150 1914 200 — 249. 250 300 350 i ] 14 Fih i ran t ■ i f i-, >■ i [ ■ i i i [ i i i i । । 400 450 500 550 Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73
5000 TIIn 147 34.00 34.20 34.40 34.60 m/z 221.05 26.39% . । 211 ; । . 21 । . 327 , ,. 415, , 519,561 miz—> 50 100* 150 200 250 ’ 300 350 400 450 500 * 550 Abundance #71006. Ethanedioic acid, bis(trimethylsily!) ester 73 ... qi ’ (’ IPi l]' I I I I I I 147 34.00 34.20 34.40 34.60 5000 m/z 281.00 13.92% 45 • ‘ i ' ‘ 117 ' I 1 1 1 1 I 1 ,190200219 250 ,,,,,, ..' 300 ........ ' ‘ 350 ‘ ‘466 ‘ ‘ 450 ‘ ‘ 500 ‘ ' 550 ' miz-> 50 100 150 Abundance #71782: Butanoic acid, 3-methyl-2-[(trimethylsilyl)oxy]-, t -PP-ee= 73 34.00 34.20 34.40 34.60 145 m/z 355.0 13.24% 5000
45 190 219 247 TB8nB/m—B122-03*me —nBTIvr 1 i • ' ' ' I ‘ ■ I ‘ r1 1 1 1 1 1 1 I ' m/z—> 50 100 150 200 250 300 350 400 450 500 550 34.00 34.20 34.40 34.60
30645.D GCMS1126.M Fri Feb 01 10:53:28 2002 Page 14
NYC-WTC_000018488
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NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
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NYC-WTC_000018416
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
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NYC-WTC_000018417
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
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NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
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NYC-WTC_000018436
Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.
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NYC-WTC_000018440
Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.
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