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GCMS analysis results for sample AD31074, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD31074 conducted on January 18, 2002, noting no unusual compounds were detected.

NYC-WTC_000017405–000017433

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0 802\31074.D Vial: 12 Acq On 9 Jan 2002 12:04 am Operator: 209 GALOS Sample gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 16 Ethanedioic acid, bis(trimethy Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T. 31.56 1.83 ug/1 414248 Chrysene-dl2 32.84

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethanedioic acid, bis(trimethylsily 234 C8H18O4S12 018294-04-7 32 2 Trisiloxane, 1,1,1,5,5,5 -hexamethyl 384 C12H3604Si5 003555-47-3 32 3 2-Hexene oic acid, bis(trimethylsi 288 C12H24O4Si2 055494-10-5 23 4 Butanoic acid, 3-methyl-2-[(trimeth 262 C11H26O3S12 055124-92-0 23 Abundance 7 Scan 2889 (31.563 mln): 31074.D (-) m/z 73.00 1 00.00% 73

5000 147 221 355 281 429 31.20 31.40 31.60 31.80 45 I 96 117 1i iiffriqn .“.1.1.11., 1911 1 , Tamnpodn) 325 Tfmmmntmtr li... 401 mh 249 „ j t m/z 147.00 41.10% m/z->__ 406080 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance’ #71006: Ethanedioic acid, bis(trimethylsily!) ester 73

5000 147 ... a.... 31.20 31.40 31.60 31.80 m/z 221.05 24.44% 45 117 । 190 219 TIEPppT > 11 > > > ■ । 11Y■11T11111 11 । 11 > 111 > > ■ । । । ■i11।111(।11 11 11 i i i । > 11 > । ।« । । ।।!i>111111 11 > i >>] i m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance ‘ : y b 73 147 31.20 31.40 31.60 31.80 5000 m/z 281.00 16.67% 281 45 369 117 207 249 1' *' * I ।....।....।....।....।.... ।.... ।.... j.... ।. m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #40777:2-Hexenedioic acid, bis(trimethylsilyl) ester, (E)- " " i i " ■ ■ i ' 73 31.20 31.40 31.60 31.80 m/z 206.95 10.83% 5000 147 45

___ 1 , i J 112 244 273 - AA - ------ . ' A • • _ -A ■ “' I' ‘ "IIT ’d8 . . T I .... | I ! I -I | I ... | . m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 1 31.20 31.40 31.60 31.80

31074.D GCMS0103.M Wed Jan 09 12:25:22 2002 Page 16

NYC-WTC_000017428

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NYC-WTC_000017428Source: NYC Law Department, mirrored locally

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