NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\JAN0 802\31074.D Vial: 12
Acq On 9 Jan 2002 12:04 am Operator: 209 GALOS
Sample gems scan 12/20 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 16 Ethanedioic acid, bis(trimethy Concentration Rank 10
R.T. EstConc Area Relative to ISTD R.T.
31.56 1.83 ug/1 414248 Chrysene-dl2 32.84
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Ethanedioic acid, bis(trimethylsily 234 C8H18O4S12 018294-04-7 32
2 Trisiloxane, 1,1,1,5,5,5 -hexamethyl 384 C12H3604Si5 003555-47-3 32
3 2-Hexene oic acid, bis(trimethylsi 288 C12H24O4Si2 055494-10-5 23
4 Butanoic acid, 3-methyl-2-[(trimeth 262 C11H26O3S12 055124-92-0 23
Abundance 7 Scan 2889 (31.563 mln): 31074.D (-) m/z 73.00 1 00.00%
73
5000 147
221
355 281
429 31.20 31.40 31.60 31.80
45 I 96 117
1i iiffriqn .“.1.1.11.,
1911 1 ,
Tamnpodn)
325
Tfmmmntmtr li... 401 mh
249 „ j t
m/z 147.00 41.10%
m/z->__ 406080 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420
Abundance’ #71006: Ethanedioic acid, bis(trimethylsily!) ester
73
5000
147
... a....
31.20 31.40 31.60 31.80
m/z 221.05 24.44%
45
117 । 190 219
TIEPppT > 11 > > > ■ । 11Y■11T11111 11 । 11 > 111 > > ■ । । । ■i11।111(।11 11 11 i i i । > 11 > । ।« । । ।।!i>111111 11 > i >>] i
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance ‘ : y b
73
147
31.20 31.40 31.60 31.80
5000 m/z 281.00 16.67%
281
45 369
117 207 249
1' *' * I ।....।....।....।....।.... ।.... ।.... j.... ।.
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #40777:2-Hexenedioic acid, bis(trimethylsilyl) ester, (E)- " " i i " ■ ■ i '
73 31.20 31.40 31.60 31.80
m/z 206.95 10.83%
5000
147
45
___ 1 , i J 112 244 273 - AA - ------ . ' A • • _ -A
■ “' I' ‘ "IIT ’d8 . . T I .... | I ! I -I | I ... | .
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 1 31.20 31.40 31.60 31.80
31074.D GCMS0103.M Wed Jan 09 12:25:22 2002 Page 16
NYC-WTC_000017428
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