NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30713.D Vial: 28
Acq On 1 Jan 2002 3:07 pm Operator: 209 GALOS
Sample gems scan 12/19 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 11 2-Hexenedioic acid, bis(trimet Concentration Rank 10
R.T. EstConc Area Relative to ISTD R.T.
31.72 0.39 ug/1 102071 Chrysene-dl2 33.02
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Hexenedioic acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 23
2 trans-3-Hexenedioic acid, bis(trime 288 C12H2404Si2 000000-00-0 23
3 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 23
4 1,1,1,5,7,7 77-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 13
Abundance Scan 2905 (31.716 min): 30713.D (-)
73
5000 147
221
355 ... 281
31.40 31.60 31.80 32.00
mpmat TTpm .... 1911, mHmTT
45 95 1 327. -44Ppkp
129 ,
m/z 147.00 40.03%
miz-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #40777:2-Hexenedioic acid, bis(trimethylsily!) ester, (E)-
l 73
5000 ■ 1 i ■ ■ • 1 i ■ ■ ‘ 1 i ■ ■ 1 ‘ i ‘ ■ i
147 31.40 31,60 31.80 32.00
45 m/z 221.05 21.55%
J 112 244 273
LU T p7. > p... ।.... p... p... (1... p.p...p.. .p...p... p... p.. >p... p ■.. p
•••‘r ‘'‘I
miz-> 40 60 80 100120140160180200220240260280300320340360380400420
[Abundance #40770, trans-3-Hexenedioic acid, bis(trimethyisilyl) ester
i 73
3140 31.60 31.80 32.00 1
5000 m/z 281.00 15.43%
147
45
,: 112 244 273
'....p’...p...p ...’p.. .-p .p’.’.. t i।>i।p।t....j....t... i (t... 11 ■...j।p
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420
A
Abundance #30580: Ethanedioic add, bis(trimethylsilyl) ester
73 147 31.40 31.60 31.80 32*00 ‘ '
m/z 207.00 11.35%
5000
45
AMAWWMW AN/
! 190 219
Tgur TDTTTTT TIITTWTTWTTTMTUITTIOTPTOITOIWTITUTTDTTTTT
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 31.40 31.60 31.80 32.00TTT
30713.D GCMS1126.M Wed Jan 23 08:47:07 2002 Page 11
NYC-WTC_000018172
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