GCMS analysis results for sample AD31018, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

‘Data File C:\HPCHEM\1\DATA\JAN0 802\31018.D Vial: 14 Acq On 9 Jan 2002 2:01 am Operator: 209 GALOS Sample gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table . Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Ethanedioic acid, bis(trimethy Concentration Rank 15 R.T. EstConc Area Relative to ISTD R.T.

34.22 0.75 ug/1 146376 Chrysene-dl2 32.83

Hit# of 5 Tentative ID MW MolForm CAS# Qual I Ethanedioic acid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 38 2 3-(3-Hydrpxyphenyl)-3-hydroxypropio 398 C18H3404S13 000000-00-0 37 3 3-Isopropoxy-1, 1,1,7,7, 7-hexamethyl 576 C18H5207Si7 071579-69-6 33 4 Trisi xane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 32 Abundance Scan 3178 (34.219 min): 31018.D (-) m/z 73.00 100.00% 73

5000 147 221 - FPTPAT 1m r r

K 281 355 33.80 34.00 34.20 34.40 34.60

m/z-> 43 TTIT . . 50 100 150 191 200 250 -2 4 4012 300 350 400 450 500 550 m/z 147.00 44.16% Abundance #71006: Ethanedioic acid, bis(trimethylsily!) ester 73

147 5000 33.80 34.00 34.20 34.40 34.60 45 190 219 m/z "7 27.05% 117 miZ-? 50 100 150 200 250 300 350 40 450 500 550 Abundance ■1 ' Hvt. 11 - ' . mpropjo ■ . : 1 73 267

33.80 34.00 34.20 34.40 34.60 5000 147 m/z 281.00 18.43% 207 398 47 293 341 m/z-> 50 100 150 200 250 300 350 _400 450 500 550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim —11181141 A / IM A,AA A NAA 73 33.80 34.00 34.20 34.40 34.60 m/z 355.05 14.87% 5000 147 221 281 297 415 I l 327 L 519 561 I 1 1 ITT1 r ■ । | ■ l ■ 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 33.80 34.00 34.20 34.40 34.60

31018.D GCMS0103.M Wed Jan 09 12:08:32 2002 Page 14

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