NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 23 pages
GC/MS analysis results for sample AD30909, Jan 28 2002
Machine-extracted title · confidence 100%Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
NYC-WTC_000018693–000018715Folder label: “GCMS X 12/19/01 A 1/2/02”
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OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30909.D Vial: 52 Acq On 2 Jan 2002 4:19 pm Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 1-Monolinoleoylglycerol trimet Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
30.25 1.82 ug/1 371650 Chrysene-dl2 33.03
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404S12 054284-45-6 42 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 23 3 1,1,1,5,7,7,7-Hepuamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 23 4 Benzoic acid. ,4-bis[(trimethylsil 370 C16H3004Si3 010586-16-0 16 Abundance Scan 2745 (30.247 mln): 30909.D (-) m/z 72.9,5 100.00% 73
5000 147 221 TBI 1 ' i ■ ■ ■ • i ' ' 281 355 30.00 30.20 30.40 30.60 45 _ 1 ‘i ' i 96 117 .. 1911 . 251 1,, , 327, L 401 429 r ■ r । ■ . m/z 146.9 34.75% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73
207 5000 147 30.00 30.20 30.40 30.60 34 m/z 221.0 103 281 20.00% 395 i • 482 • 414** + 1 41*11**$* ' ■ i ' ' ■ 1 mz-> 50 100 150 200250 300 350 '460 450 Abundance #52459; Trisiloxane, 1,1.1,5,5.5-hexamethyl-3.3-bis[(trimet 73 147 ............ ...................... 281 30.00 30.20 30.40 30.60 5000 m/z 281.00 13.20% : I 369 i 207 249 ( i 338 i • ■ i PP—It 1 ‘ I 1 1 • 1 I 1 1 1 1 1 1 ' miz-> 50 100 150 200 250 300 350 400 450 Abundance #56714: 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 30'00 30.20 30.40 30.60 m/z 355.0 12.72% 147 5000 267 355 429 45 207 • ■! ■ ■ ' ‘ I ■ ■ ' 1 1 • • ■ ■ i ■ ■ ■ ‘ i ■ • • ■ I • ■ ‘ r I ■ ■ ■ ■ i ‘ 5*1 1 ' 1 m/z-> 50 100 150 200 250 300 350 400 450 30.00 30.20 30.40 30.60
30909.D GCMS1126.M Fri Jan 25 11:40:45 2002 Page 11
NYC-WTC_000018710
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NYC-WTC_000018710Source: NYC Law Department, mirrored locally
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