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GCMS analysis results for sample AD31074, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD31074 conducted on January 18, 2002, noting no unusual compounds were detected.

NYC-WTC_000017405–000017433

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017430
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0 802\31074.D Vial: 12 Acq On 9 Jan 2002 12:04 am Operator: 209 GALOS Sample gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 18 1-Monolinoleoylglycerol trimet Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

34.22 1.27 ug/1 287625 Chrysene-dl2 32.84

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404S12 054284-45-6 45 2 Trisiloxane, if, 1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 32 3 Ethanedioic acid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 32 4 Butanoic cid, 3-methyl-2-[(trimeth 262 Abundance" 73

147 Scan 3178 (34.216 mln): 31074.D (-) C11H26O3S12

m/z " T 055124-92-0 23

5000 221 281 355 33.80 34.00 34.20 34.40 34.60 45 96 117 TTIr TITT Mu i 191 L-- rr1" . I . . 327, ! ■ . 401 42% m/z 147.00 44.66% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 33.80 34.00 34.20 34.40 34.60 34 103 281 m/z 221.05 25.30% t I l: I 395 482 ■ • i ■ m/z-> 50 100 150 200 250 300 350 400 450 Abundance 73 147 33.80 34.00 34.20 34.40 34.60 5000 m/z 281.00 15.45% 281 45 369 ■ ■ ■ i ■ 117 ,207.249............................. m/z--> 50 100 150 200 250 300 350 400 450 - Abundance #71005: Ethanedioic acid, bis(trimethylsilyl) ester 73 33.80 34.00 34.20 34.40 34.60 m/z 355.0 12.23% 147 5000

45 I i dr 117 j 190 219 ■ ■ ■ ‘ r* 1 1 ‘ I ‘ ‘ ‘ ‘ I ‘ ‘ 1 * I ' 1 m/z-> 50 ' 100 150 200 250 300 350 400 450 33.80 34.00 34.20 34.40 34.60

31074.D GCMS0103.M Wed Jan 09 12:25:31 2002 Page 18

NYC-WTC_000017430

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NYC-WTC_000017430Source: NYC Law Department, mirrored locally

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