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GC/MS analysis results for sample AD30935, Jan 28 2002

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Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.

NYC-WTC_000018754–000018774

Folder label: “GCMS X 12/19/01 A 1/2/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30935.D Vial: 48 Acq On 2 Jan 2002 11:27 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 1-Monolinoleoylglycerol trimet Concentration Rank II R.T. EstConc Area Relative to ISTD R.T. 34.37 0.30 ug/1 73061 Chrysene-dl2 33.02 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1 -Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 42 2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 35 3 3-Isopropoxy-1/1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 33 4 3-Trimethylsilyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 23 Abundance Scan 3195 (34.373 min): 30935.D (-) 73

147 5000 221 281 355 429 —""1 +144 . 327 [ 34.00 34.20 34.40 34.60 34.80 m/z 147.00 49.91%

1 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000- 147 34.00 34.20 34.40 34.60 34.80 34 103 281 m/z 221.05 29.14% Il I I 11 H I - . 395, ...482 ........ miz-> 50 100 150 200 250 300 350 ' ‘ 400 " 450 ‘ ' 500 ‘ ' 550 Abundance #71006 Ethanedicic acid, bis(trimethylsilyi) ester 73

147 34.00 34.20 34.40 34.60 34.80 5000 m/z 281.00 18.62% 45 117 190 219 —Ihm—PP m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim » j • IT l*| TI 1 1 | ’1-4] \ "ITTTB* 73 34,00 34,20 34.40 34.60 34.80 m/z 354.9,5 15.64% 5000 147 221 281 415 J___ 1_ 327 i 519 561 miz-> 50 100 150 200 250 300 350’* 400 ' 450 500 ' 550 ‘ ■ । ■1 ■ ■ । ■1 ■ ■ ।11 *11111111 34.00 34.20 34.40 34.60 34.80

30935.D GCMS1126.M Fri Jan 25 11:51:09 2002 Page 13

NYC-WTC_000018773

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NYC-WTC_000018773Source: NYC Law Department, mirrored locally

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