GCMS analysis comments, sample AD29231, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC2701\29231.D Vial: 57 Acq On 30 Dec 2001 3:05 pm Operator: 209 GALOS Sample GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C : \DATABASE\NBS75K . L ********************************************************************* Peak Number 13 1-Monolinoleoylglycerol trimet Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

31.71 0.67 ug/1 705410 Chrysene-dl2 33.05

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 45 2 3-Isopropoxy-1,1,1,7, 7/7-hexamethyl 576 C18H5207Si7 071579-69-6 40 3 Ethanedioic acid, bistrimethylsily 234 C8H18O4Si2 018294-04-7 32 4 2-Hexenedioic acid, ^is(trimethylsi 288 C12H2404Si2 055494-10-5 23 Abundance i Scan 2905 (31.711 min): 29231.D (-) m/ z 73.00 100.00% 73

5000 147 221 .............. ......................... 281 me 31.40 31.60 31.80 32.00 45 T TT 117 ‘ r , 1911 _ । ' । r |"i TT 249, . 3271 401 429 ............ m/z 147.00 39.89% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 / 5000 147 31.40 31.60 31.80 32.00 34 103 281 m/z 221.05 22.48% I I — — 325 -2 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503; 3-Isopropoxy-1 .1.1.7.7.7-hexamethyl-3,5,5-tris(trim 73 / TI" 31.40 31.60 31.80 32.0G 5000 m/ z 2 81.00 15.08% 147

m/z-> 1 1 ' 50 I

100 . 212 327, . .415.... 561 150 200 250 300 350 400 450 500 550 Abundance #30580: Ethanedioic acid, bis(trimethylsilyl) ester ----- I 73 147 31.40 31.60 31.80 32.00 m/z 355.0 9.93% 5000 45

ll 120 219 ■ • । • < ■ ■ । m/z--> 50 100 150 200 250 300 350400 450500 550 31.40 31.60 31.80 32.00

29231.D GCMS1126.M Mon Dec 31 14:00:01 2001 Page 13

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