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GC/MS analysis results for sample AD30935, Jan 28 2002

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Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.

NYC-WTC_000018754–000018774

Folder label: “GCMS X 12/19/01 A 1/2/02

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NYC 9/11 Public Portal Document

Tentatively Identified Compound (LSC) summary

Operator ID: 209 GALOS Date Acquired: 2 Jan 2002 11:27 am Data File: C:\HPCHEM\l\DATA\DEC3101\30935.D Name: gems scan 12/19a Mise: Method: C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title: 209 625/TCLP calibration table Library Searched: C:\DATABASE\NBS75K.L

TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc

Silane, tetramethyl- 7.61 4.1 ug/1 1084270 ISTD01 11.68 5319450 20.0 Cyclotetrasiloxane,/ 11.13 0.3 ug/1 77778 ISTD01 11.68 5319450 20.0 Cyclopentasiloxane. 14.30 1.8 ug/1 569671 ISTD02 15.28 6504220 20.0 1,1,1,5,7,7,7-Heptam 17.45 3.5 ug/1 1126590 ISTD02 15.28 6504220 20.0 Furan, tetrahy o-2. 18.16 0.3 ug/1 97476 ISTD03 20.56 7288230 20.0 Trisiloxane, 1<1,1,5 20.28 2.3 ug/1 822746 ISTD03 20.56 7288230 20.0 Benzoic acid/ 4-etho 21.06 1.2 ug/1 447882 ISTD03 20.56 7288230 20.0 N- (Trifluoroacetyl) - 22.79 1.4 ug/1 515651 ISTD04 24.98 7219450 20.0 3-1 sopropoxy- 1,1,1,7 26.89 0.7 ug/1 240853 ISTD04 24.98 7219450 20.0 Trisiloxae, 1,1,1,5 28.65 0.5 ug/1 175665 ISTD04 24.98 7219450 20.0 3-Isopropoxy-1, 1,1,7 30.25 0.6 ug/1 143347 ISTD05 33.02 4834960 20.0 1,1,1,5,7,7,7-Heptam 31.72 0.5 ug/1 120565 ISTD05 33.02 4834960 20.0 1-Monolinoleoylglyce 34.37 0.3 ug/1 73061 ISTD05 33.02 4834960 20.0 / 30935.D GCMS1126.M Fri Jan 25 11:51:09 2002

NYC-WTC_000018774

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NYC-WTC_000018774Source: NYC Law Department, mirrored locally

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