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GCMS analysis log for sample AD31073

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

NYC-WTC_000017434–000017458

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017450
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OCR status: ocr · source: ours

NYC 9/11 Public Portal Document _ Library Search Compound Report “|. + "Data File : C:\HPCHEM\1\DATA\JAN0802\31073.D Vial: 10 Acq On : 8 Jan 2002 10:07 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESS IOI IGE IO IIIS IOC IIIT IOUS ITSO IOEI I TORI ISO TIO III IOI II II IE Peak Number 9 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 10 R.T. EstCone Area Relative to ISTD R.T, 26.73 1.28 ug/1 439680 Phenanthrene-d10 24.80 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 3-Isopropoxy~1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 56 2 1-Monolinéleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 33 3 Mercaptéacetic acid, bis(trimethyls 236 C8H2002SSi2 006398-62-5 28 4 Mande¥ic acid ditbdms == 380 C20H36038i2 _078324-07-9 25 ‘Rbundance ‘Scan 2362 (86.783 miny: 31073. G) m/z 73.00 100.00% i | ' 5000: | 447 J | . el 355 491 429 _"2640_26.60 26.80 27.00" ater eh PL 248 Sei AO m/z 147.00 32.35% mz 50 100150200250. 300. _360_400__450__500__550_| h { Abundance 60803: Feopropony-1,1..7,7.7 Rexamatiy-3 BS. i} | % | 5009) | 147 LL ae '28.60_26.80_27:00 m/z 281.0 14.88 21-281 507 ny 519 eat mz-> 50. 100. 150-200-250 300-380-400. 450500 550 ‘Abundance Ey 207 26.40 26.60 26.80 27.00 5000. 147 m/z 221.05 "14.38 “ 103 | 281 a | . a! 482 | mz->___ 60 100 150__200__250_300__350_400__450 500 __ 550. Abundance #30848: Mercaptoacatic acid, bis(trimethyisilyl)- 7 Pas 2640 26160 26.80 27100 Tm/z 74.00 8.218 | 221 } #8 soy 199 | me-> ‘50100150 200 250300 350 400. 450 500 550 26.40 26.60 26.80 27.00 31073.D GCMS0103.M Wed Jan 09 12:19:33 2002 Page 9 NYC-WTC_000017450

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NYC-WTC_000017450Source: NYC Law Department, mirrored locally

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