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GCMS analysis log for sample AD31073

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

NYC-WTC_000017434–000017458

Folder label: “GCMS X 12/20/01 A 1/8/02”

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Scanned page image, NYC-WTC_000017449
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NYC 9/11 Public Portal Document * <th Library Search Compound Report “|. + ‘Data File : C:\HPCHEM\1\DATA\JAN0802\31073.D Vial: 10 Acq On : 8 dan 2002 10:07 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JERE ISIE ISS IOI II IOSI ISO IODISI ODI ITI IOEI ITO III I III Peak Number 8 Benzeneethanamine, N-[(pentafl Concentration Rank 6 R.T. EstCone Area Relative to ISTD R.T. 22.64 2.87 ug/1 985113 Phenanthrene-d10 24.80 Hit# of 5 Tengative ID MW MolForm cAS# Qual 1 Benzeneethanémine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 27 2 Benzoic ag#4, 2,5-bis(trimethylsilo 370 C16H3004Si3 003618-20-0 25 3 N-(Trifls6racetyl) -0,0',O"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 25 _4 3-Isopr6poxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 23 ‘Abundance ‘Scan 1816 (22.636 min): 31073.D (-) jw 73.00 100.00: | | 5000: ma 7 01 2240 22.60 22160 23.00 45 4 180 22.60 23: Pan Ph bg eh ent tt m/z 147.00 26.00 miz->__50__ 100 __150__200__250 __300__350__ 400 450 __500__550__| uica °° —"Sraos anconsabonie Nope ice I 7B 355 } | | | aes |__"""calao’ "22160" 22:80 23.00 iy | m/z 355.05 25.10 Lt 208251 261 386, 458. 548 i mz> "80 100” 150. 200 250 300° 350 400-450 600850 I | ‘Abundance Ea) 255, 22.40 22.60 22.80 23.00 15000: m/z 221.05 19.13% 45 147 479 228 287 207 | ' miz> ____50__ 100 150__ 200.250.300.350 _400__450_500__ 50 \ | Abundanios #58807: N-(Trifivoraceiy)-O,0" O™tis(timethylaiy)epin errr fhcprre | ] __22.40 22.60 22.80 23.00 | 355 m/z 281.00 14.62% \ | vi 140184 281 490_ . | mz» 5 100 180-200. 250 300380 400. 400500 580 22.40 22.60 22.80 23.00 31073.D GCMS0103.M Wed Jan 09 12:19:29 2002 Page 8 NYC-WTC_000017449 7

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NYC-WTC_000017449Source: NYC Law Department, mirrored locally

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