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GCMS analysis log for sample AD31073

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

NYC-WTC_000017434–000017458

Folder label: “GCMS X 12/20/01 A 1/8/02”

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Scanned page image, NYC-WTC_000017448
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NYC 9/11 Public Portal Document : Library Search Compound Report “. + ‘Data File : C:\HPCHEM\1\DATA\JAN0802\31073.D Vial: 10 Acq On : 8 Jan 2002 10:07 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESS SISSIES SCISSORS SSIS TOSI ISDS IGT SEI SSSIS SSCS ISTO SIGS ISHII ISIE Peak Number 7 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 8 R.T. EstCone Area Relative to ISTD R.T. 20.85 1.52 ug/l 497744 Acenaphthene-d10 20.39 Hit# of 5 Tenpative ID MW MolForm cas# Qual Benzoic acig/ 4-ethoxy-, ethyl este 194 C11H1403 023676-09-7 97 2 1-Pentanopé, 1-(4-hydroxyphenyl)- 178 C11H1402 002589-71-1 43 3 Benzoic Acid, ethoxy-, ethyl ester 194 C11H1403 075333-22-1 43 4 Benzojé acid, 2-hydroxy-, hydrazide 152 C7H8N202__—=—(000936-02-7 43 ‘Abundance ‘Scan 1721 (20.847 min: 31078.) ~T m/z 20 200-008 121 | \ 5000: 149 6 «s 138 194 39 196 20.60_20.80_21.00_21.20 50. 78 Seana nte 78 we 149-09 46.98 miz->__20 30 40 50_60_70_80_90 100 140 120 130 140 180 160 170 180 190 200 Abundance W212: Benzdic ace, ethoxy, ety ester | 1 149 | tad 138 “98 20.60 20.80 21.00 21.20 7 8 9 ae m/z 180 26.26) miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 i ‘Abundance ra | 121 5000. m/z 194.0 25.958 65 93 | i 39 53 ” 88 193 \ miz->_ 2030.40.80 60.70.80 90.100 110 120 130 140. 160 160 170 180 180 200. Abundance #21246; Benzoic acid, ethoxy-, ethyl ester 7 } 181 20.60 20.80 21.00 21.20 m/z 64.9 21.78% 138 5000. 39 | | 198 _ | | miz-> 20 30 40 50 60 70 80 90 “Oo 10 120 150 140 180 160 170 180 100 200 | 20.60 20.80 21.00 21.20 | 31073.D GCMS0103.M Wed Jan 09 12:19:24 2002 Page 7 NYC-WTC_000017448 ‘

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Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31024 performed on January 18, 2002.

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