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GCMS analysis log for sample AD31073

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

NYC-WTC_000017434–000017458

Folder label: “GCMS X 12/20/01 A 1/8/02”

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Scanned page image, NYC-WTC_000017447
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OCR status: ocr · source: ours

NYC 9/11 Public Portal Document ae Library Search Compound Report “| + "Data File : C:\HPCHEM\1\DATA\JAN0802\31073.D Vial: 10 Acq On : 8 Jan 2002 10:07 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L rereerrrrrrrr teres sttrrrrr strc rerrtrrrrrrrtrr ttt ttt ttt rrr itr r ctr! Peak Number 6 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 20.12 4.78 ug/1 1564890 | Acenaphthene-d10 20.39 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 Trisiloxane, 7,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 42 2 4-Amino-5-ipfidazole carboxamide, tr 342 C13H30N40Si3 000000-00-0 10 3 Octadecanofe acid, 2-[(trimethylsil 386 C22H4603Si 056196-58-8 9 4 Phosphoric acid, 2-(methoxyimino) -3 415 C13H34NO6PSi3__055319-85-2 9 Roundance ‘Sean 4642 (20.122 ming: 310730 C) | m/z = 100. 00% 5000: | ar 281 45 Ea wr, 18 | 19.80_20.00 20.20 20.40 _ 0 98 AT het 18 archer oer 38S Beamer | m/z 147.00 33.64 iz» ___40_60_80_100 120 140 160 180.200 220 240 260 280 300 320 340 360 380 400.420. | Abundance Jp ReMse Teale, 11.1 Shomamety [net | 147 | = 5000: | ‘49.80 20.00 20.20.2040 369 [m/z 281.0 27.93% 207 4g a | mz-> 40 60 80 100 120 140 160 180 200 220 240 260 260 300 320 340 360 380 400 420 | | ‘Abundance : | 73 | 5000 m/z 326.9 10.66 2a7 4s | 147 72 22288 | infz->___"40 80. 80.100 120 140 180 180 200 280 240 280 280 300 320 940 960 80 400 420 Abundance ‘#74126: Octadecanolc acid, 2-[(irimethylsilyljoxy]-, methyi + 4 19.80 20.00 20.20 20.40 | a7 m/z 74.00 8.49) | | 199 129 150 Be miz—> ‘40 60 60 a | 19.80 20.00 20.20 20.40 31073.D GCMS0103.M Wed Jan 09 12:19:20 2002 Page 6 NYC-WTC_000017447

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NYC-WTC_000017447Source: NYC Law Department, mirrored locally

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