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GCMS analysis log for sample AD31073

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

NYC-WTC_000017434–000017458

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017446
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NYC 9/11 Public Portal Document Lot, Library Search Compound Report “| + “Data File : C:\HPCHEM\1\DATA\JAN0802\31073.D Vial: 10 Acq On : 8 dan 2002 10:07 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESSIE SISSIES ISI IIE EIS ISS IS EIS IS IIE ISIIO ISS ISIE IS ISI IOI IIT Peak Number 5 2-Propanone, 1-(1-methylethoxy Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 18.00 0.47 ug/1 153033 Acenaphthene-d10 20.39 Hit# of 5 Tentayive ID MW MolForm cas# Qual 1 2-Propanone, j“(1-methylethoxy) - 116 Cé6H1202 042781-12-4 37 2 Sinalbin 424 C14H18NO10S2 027299-07-6 14 3 Furan, tefahydro-2,2,5,5-tetrameth 128 C8H160 015045-43-9 12 4 2-Heptayéne 114 c7H140 000110-43-0 10 Abundance 7 ‘Scan 1411 (18.002 min): 31073.0 ¢) m/z 43.00 100.00% | % 73 am 414 | 95 a ee 17.60 17.80 18.00 18.20 18.40 She seek 8] m/z 57.00 65.55% man>__20__ 3040506070 _80__90_100_110 120 190 140_180_ Abundance RAE RPropanoks, -(Tmenyenonyr | | 5000: | 47.60 17.80 18.00 18.20 18.40 ar | 5B 73 (m/z 73.00 55.53% mi» 2030 40.80. 6070. 80. 90 100 110 120 130 140 150. | Abundance 43 78 a 106 133 17.60_1780 18.00 18.20 18.40 600: st m/z 111. 36.42 al " | \ | mig» 209040. 9060. 70.8090. 100110 120180. 140.150. Abundance #65056: Furan, tetrahydro-2,2.5,5-tetramethyl- + | ° [17.60 _17.80_18.00 18.20 18.40 | | m/z 69.00 25.42 5000 | | $5 | ] 70 us ae 95 miz-> 20 30 40 50 60 70 80 9 100 110 120 130 140 150 17.60 17.80 18.00 18.20 18.40 31073.D GCMS0103.M Wed Jan 09 12:19:15 2002 Page 5 NYC-WTC_000017446

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NYC-WTC_000017446Source: NYC Law Department, mirrored locally

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Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31076 on January 18, 2002.

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Laboratory note stating that the GCMS scan of sample AD31017 did not reveal unusual compounds on January 18, 2002.

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GCMS analysis log for sample AD31024 · Box DEP Box 16

NYC-WTC_000017494

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31024 performed on January 18, 2002.

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