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GCMS analysis log for sample AD31073

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

NYC-WTC_000017434–000017458

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017445
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NYC 9/11 Public Portal Document Loe Library Search Compound Report - + ‘Data File : C:\HPCHEM\1\DATA\JAN0802\31073.D Vial: 10 Acq On : 8 Jan 2002 10:07 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ee VeOwrrrrrrr rr srrerererrerrrrrrrrtrrrttr rt tri t rit irr r irri roti rol Peak Number 4 Cyclohexasiloxane, dodecamethy Concentration Rank 1 R.T. EstCone Area Relative to ISTD R.T. 17.30 7.39 ug/1 2290580 = Naphthalene-ds 15.12 Hit# of 5 Tentative ID MW MolForm cAS# Qual 1 Cyclohexasiloyéne, dodecamethyl- 444 C12H3606Si6 000540-97-6 38 2 2H-1,4-Benzg@iazepin-2-one, 7-chlor 342 C18H19C1N20Si 055299-24-6 16 3 1,1,1,5,7/7,7-Heptamethyl-3,3-bis(t 444 C13H4005Si6 038147-00-1 16 _4 Silane, (1,2,3-benzenetriyltris (oxy 342 C15H3003Si3___017864-23-2 16 Abundance — * ‘Scan 1336 (17-304 min): 3073.0 ¢) m/z oh 100.008 M44 147 ae 4 207: i 42a | 47.00 17.20 17.40 17.60 i 96 117 179, 20720 251 201311 27 ae aa 37-318 miz->___40 6080 100.120 140 160 180200 220 240 260 280 300 320 340 360 380 400 420.440 ‘Abundance #56711: Cyclohexesiloxane, dodecamethyl- | | ii on | } 429 5000] | | ‘17100 47:20. 17:40 _ ] a7 m/z 147.00 "13.86% hon Bloc een re SY \ | miz-> __" 40. 60. 80 100120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440 | 3 aa ] 17.00 17.20 17.40 17.60 5000 | m/z sal 9.23 45 a1 116 46 27289 sig | mlz» __"aO 60. 80,100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440, Abundance #56714; 1,1,1,5.7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t + - = _17.00_17.20_17.40_17.60___| | m/z ara aay “7 | 267 | os —— ‘oe 45 | 207 ] miz-> "#0. 60 80 100120 140 160 180 200 220 240 260 280 300 320.940 360 360.400 420440 17.00 17.20 1740 1760 | 31073.D GCMS0103.M Wed Jan 09 12:19:10 2002 Page 4 NYC-WTC_000017445

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NYC-WTC_000017445Source: NYC Law Department, mirrored locally

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