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GCMS analysis log for sample AD31020

Machine-extracted title · confidence 95%

Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31020 on January 18, 2002.

NYC-WTC_000017459–000017477

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017472
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NYC 9/11 Public Portal Document ; . Library Search Compound Report ‘+ “Data File : C:\HPCHEM\1\DATA\JAN0802\31020.D Vial: 15 0 Acq on : 9 dan 2002 2:59 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title + 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peereetrerrrrrrerrrr Trt rrererrrrrrertrrr rrr itt rit titi titi rt ri rtr tri ty Peak Number 7 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 7 R.T. EstCone Area Relative to ISTD R.T. 20.85 1.05 ug/1 324311 | Acenaphthene-d10 20.39 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzoic acid, 4-ethoxy-, ethyl este 194 C11H1403 023676-09-7 97 2 Ethyl 3-hydroxybenzoate 166 C9H1003 007781-98-8 38 3 Benzenepropanoic acid, 4-methoxy-, 194 C11H1403 015823-04-8 38 4 Benzoic acid, ethoxy-, ethyl ester 194 C11H1403 075333-22-1 38 Abundance = “Scan 1722 (20.850 min): $1020.D (-) m/z an 100.00% 181 ‘5000 149: i | 6 P 138 va es 39 166 20.60 20,80 21.00 21.20 50 76 P ‘ BA reer, : rotate | mz 149.00 48.248 miz->__20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 160 190 200. ‘Abundanes #21260: Benzoic acid, 4-ethoxy-, ethyl ester # | | | 149 | | | 438 | jot 20.60_20.80_21.00_21.20 ” 65 fe 1 PT ae f [im7z aan 28.13% | | | miz—> 2G 40.60 60 70 BOB) 100 110 120 10 140 180 180 170 180 700 200 | | ‘Abundance | jar —"""pol60 2ole0 241002120." | 5000 m/z 137-98 25.70% % 65 138 168 i 181 San aatmermmemantetr miz-> ___20 30 40. 50 60-70 80 90 100 110 120 130 140 150 160 170 180 190 200 | | ‘Abundance. +#24262: Berizenépropanoic acid, 4-methoxy-, methyl ester i tet 20,60 _20.80 21.00 21.20 | m/z a 21.19 5000 | 434 194 - - - 108 4151_163 miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 20.60 20.80 21.00 21.20 31020.D GCMS0103.M Wed Jan 09 12:11:50 2002 Page 7 i NYC-WTC_000017472

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NYC-WTC_000017472Source: NYC Law Department, mirrored locally

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