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GCMS analysis log for sample AD31020

Machine-extracted title · confidence 95%

Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31020 on January 18, 2002.

NYC-WTC_000017459–000017477

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017473
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NYC 9/11 Public Portal Document : . Library Search Compound Report * + "Data File : C:\HPCHEM\1\DATA\JAN0802\31020.D Vial: 15 ‘ Acq On : 9 Jan 2002 2:59 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L. Peeverwrerrrrr rrr errr Serrrrrrrrrrrtrr rt rit tr ttt rr ttt ttt ret i rrr rrr! Peak Number 8 Benzeneethanamine, N-[(pentafl Concentration Rank 6 R.T. EstCone Area Relative to ISTD R.T. 22.64 1.42 ug/1 439329 Phenanthrene-d10 24.81 Hit# of 5 Tentative ID MW MolForm caSs# Qual 1 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 25 2 N-(Trifluoracetyl) -0,0',O"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 25 3 N-(Trifluoroacetyl) -N,0,0',O''-tetr 553 C22H42F3NO4Si4 000000-00-0 22 4 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H3004Si3 003618-20-0 13 ‘Bbusdanes ‘Scan 1917 (22.640 min}: 31020.) i ahaa ary i 7 gether 7 at cu * | 22.40 22.60 22.80 ‘23,00 ro aor | 408 eee 0-2 i othe eh tly BS oh - ‘m/z 355.05 26.04 miz>____ 50100150 200__ 250 __300 350 _400__450 500 550_| ‘Abundance #74706. Benzenesthanamine, N-[(pentalvoropheryijmethyiene] | 385 | | 22.40 22.60 22.80 23.00 45 [m/z 147.90 25.05 i 208 251,281 306458 s4a_| miz-> 50. 100-150 200250 300350400450 500 580_ | ‘Abundarice eras | ‘ meme bepeeee 355, 2240 22.60 22.80 23.00 6000 m/z ai 19.13 il 140104 201 120 | Abundance #60162: N-(Trifluoroacety!)-N,O,0°,0"-tetrakis(trimethyist r 22.40 22.60 22.80 23.00 m/z 281.00 14.72% 355. if 5000) I i | | | 145) 147__ 193 267, 538 mz—> 50 100 150 200 250 300 360 400 450 500 550 22.40 22.60 22.80 23.00 31020.D GCMS0103.M Wed Jan 09 12:11:55 2002 Page 8 NYC-WTC_000017473

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NYC-WTC_000017473Source: NYC Law Department, mirrored locally

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