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GCMS analysis log for sample AD31073

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

NYC-WTC_000017434–000017458

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017456
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NYC 9/11 Public Portal Document wo Library Search Compound Report “. + "Data File : C:\HPCHEM\1\DATA\JAN0802\31073.D Vial: 10 Acq On : 8 Jan 2002 10:07 pm Operator: 209 GALOS Sample : goms scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peeeeeererrrrrrerrrt ttt ttre rrr ttrterttrrttrttt tri tt ttt ttt ttt tri t retry Peak Number 15 Decanedioic acid, bis(2-ethylh Concentration Rank 5 R.T. EstCone Area Relative to ISTD R.T. 35.42 2.92 ug/1 432663 Perylene-d12 36.90 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 Decanedioic/acid, bis(2-ethylhexyl) 426 C26H5004 000122-62-3 53 2 Butyl citrate 360 C18H3207 000077-94-1 12 3 [1,1'-Biphenyl]-4-0l, 3-amino- 185 C12H11NO 001134-36-7 10 4 Tridecéne, 7-methyl- = 198 C14H30 (026 730-14-3 10 Abundance ‘Scan 3306 (36.417 min): 31073.D ¢) m/z 185.10 100.00% 73 1! | fo 000} 5 | | me | oy AS 2a 355 35.00 35.20 35.40 35.60 35.80 168 | 20; 429 | 85: .40_35.60_ 35. Scale aa topepieereaeee pemenice ot m/z 73.00 83.36 Abundance '#55661: Decanedioic acid, bis(2-ethyiheny) ester ii \ sr - | 412 35.00 35.20 3540 35.60 35.80 | les m/z 57.90 65.188 | | 143 166 | 203 298316 rmiz-> "40. 60. 80,100 120 140 160 100 200 220 240 260 200 300 320 340 360 380 400 420 | | Abundance: F: | 185 | 129 ~ | 36.00 35.20 35.40 35.60 35.80 __ 000 m/z 70.10 49.92 . | 87 mmlz-2>___ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380400420 | | ace ston | Sphere Samo ; | 185 [35.00 35.20 35.40 35.60 35.80 | m/z 55.00. 47.52% | 000: | 186 128) miz—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 35.00 35.20 35.40 35.60 35.80 31073.D GCMS0103.M Wed Jan 09 12:20:01 2002 Page 15 i NYC-WTC_000017456

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NYC-WTC_000017456Source: NYC Law Department, mirrored locally

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