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GCMS analysis log for sample AD31073

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

NYC-WTC_000017434–000017458

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017457
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NYC 9/11 Public Portal Document ae Library Search Compound Report .. : ‘Data Pile : C:\HPCHEM\1\DATA\JAN0802\31073.D Vial: 10 Acq on : 8 Jan 2002 10:07 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESS IES IGE SSSI ISSO IIS I ISOS SOI ISOC I TORI ISI TOE TOT IOI IE Peak Number 16 Ethanedioic acid, bis(trimethy Concentration Rank 15 R.T. | EstConc Area Relative to ISTD R.T. 36.55 0.51 ug/1 75725 Perylene-d12 36.90 Hit# of 5 Tentayive ID MW MolForm CAS# Qual 1 Ethanedioic a, bis(trimethylsily 234 C8H1so4si2 018294-04-7 32 2 3-Isopropoxy+1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 3 Butanoic gid, 3-methyl-2-[(trimeth 262 C11H2603Si2 055124-92-0 23 _4 Silanamive, N-[2,6-dimethyl-4-[(tri 281 C14H27NOSi2 _072088-09-6 14 Rbundanos (Sean 3482 (B.S mine 31O7SD “—"T'n/z 73.90 100.008 | “7 | 5000: i} 2a \ 2 sol ot atta wa sale soso : ethic | m/z 147.00 57.84% miz>___§0 100 150 _200 _250 300 _350__400 450. 500.550! | ‘Abundance #71005: Ethanedioic acid, bis(timethyisilyl) ester | 147 ‘5000 | 36.20 36.40 36.60 36.80 45 | m/z 221.05 34.10% iL 117 | 190 219 | | miz-> ‘50.100 150 200 250 300. 350 400-450 500550, | | ‘Abundancé oT | 73 | 36.20 36.40 36.60 36.80 __| 5000 Pe m/z 281.00 18.07% eg Speer ile miiz->___60__100__150._200___250___300__950___400___450__500_ 580. Abundance #7178Z Butanole acid, Smethyl2-|(rimethyislyjoxyy T } Y a 8 __96.20_36.40 36.60 36.80 | 145 m/z 207.00 17,53 45 147, 190 219 247 L soe miz—> 50 100 150 200 250 300 350 400 450 500 550 36.20 36.40 36.60 36.80 31073.D GCMS0103.M Wed Jan 09 12:20:05 2002 Page 16 NYC-WTC_000017457

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NYC-WTC_000017457Source: NYC Law Department, mirrored locally

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