NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30934.D Vial: 51
Acq On 2 Jan 2002 3:21 pm Operator: 209 GALOS
Sample gems scan 12/19a Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 10 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
26.90 0.72 ug/1 229804 Phenanthrene-dl0 24.99
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 42
2 3-Isopropoxy-1,1,1, 7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40
3 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 35
4 1-MonolinoleoyXglycerol trimethylsi 498 C27H5404Si2 054284-45-6 25
Abundance Scan 2380 (26.896 mln): 30934.D (-) m/ z 73.00 100.00%
73
5000
147
221 281
26.60 26.80 27.00 27.20
45 117, , ■ 1911 I 251, ... 325,355 . 399 428 .....
TT 1* l rfi150 200 ‘ 250 ' 300 350 m/z 147.00 31.70%
m/z-> 50 100 400 450 500 550
Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet
73 147
281
_-
5000
26.60 26.80 27.00 27'20
369 m/z 281.00 20.22%
207 249 338 .......................
m/z-> 50 100 150 200 250 300 ' 350 400 450 ' 500 550
Abundance #60503: 3-sopropoxy-1,1.1, / .7.7-hexamethyl-3,5,5-tris(trim
73
—
26.60 26.80 27.00 27.20
5000 m/z 221.05 17.55%
147
221
.21 327 ..... 415......... 519 561
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bls(trimethylslloxy)t
73 26.60 26.80 27.00 27.20
m/z 207.00 8.91%
147
5000- 267
355 429
45 207
AMA Mn , 1 MAA MrrW
miz-> 50 100 150 200 250 300 350 400 450 500 550 26.60 26.80 27.00 27.20
30934.D GCMS1126.M Fri Jan 25 11:47:13 2002 Page 10
NYC-WTC_000018749
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