GCMS analysis summary, sample AD27288, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0 802\27288.D Vial: 26 Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

26.74 0.72 ug/1 247376 Phenanthrene-dl0 24.80

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trisiloxane, 1,1,1,5,5, 5-hexamethyl 384 C12H3604Si5 003555-47-3 59 2 3-Isopropoxy-1,1,1/7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 3 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 28 4 1,1,1,5,7,7,7-H tamethyl-3 /3-bis(t 444 C13H40O5Si6 038147-00-1 16 Abundance" scan 2363 (26.740 min): 27288.D (-) m/z 73.00 100.00% 73

5000 147 221 281 1 26.40 26.60 26.80 27.00 45 117 191 [ 249 [ 325 355 401 429 TT TPT 1PBTE-BmTTT**]ITTT m/z 147.00 33.96% m/z-> 50 100!__ 150 200 250 300 350 400 450 500 550 Abundance #52459: trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 281 5000 26.40 26.60 26.80 27.00 369 m/z 281.00 19.12% i 207 249. --------------------I- 338 1 m/z->_ _ 50 100 150 200 250 300 350 400 450 500 550 Abundance / r6 i ' opmpiv : ' 73 ...... .............. ......... 26.40 26*60 26.80 27.00 ‘ 5000 m/z 221.05 17.11% 147 221 281 327 415 519 561 : T’II4 m/z-> 50 100 150 200" 250 300 350 ’ 400 450 500" 550 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 141***I‘+I*** i f 1 1 1 i 73 26.40 26.60 26.80 27.00 m/z 207.00 8.59% 207 5000 147 34 103 281

imiz-> ''i1'••i' 1 't1,11r‘ 11i11 . 395, ...482 .... . . 50 100 150 200 250 300 350 400 450 500 550 26.40 26.60 26.80 27.00

27288.D GCMS1126.M Mon Feb 04 15:23:32 2002 Page 10

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