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GCMS blank analysis results

Machine-extracted title · confidence 95%

Laboratory report listing detection limits for numerous organic compounds in a GCMS blank sample analyzed on January 10, 2002.

NYC-WTC_000017344–000017363

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document nbs Library Search Compound Report “"** Data File : C:\HPCHEM\1\DATA\JAN0802\LB.D Vial: 7 Acq On : 8 Jan 2002 7:12 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESSE ISIS IES IIS EI IIE ISSO IUEI ISS ISIS III IOI TOI III IOI III IE Peak Number 9 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 12 R.T. | EstCone Area Relative to ISTD R.T. 28.50 0.59 ug/l 254199 Phenanthrene-d10 24.81 Hit# of 5 Tentatiyé ID MW MolForm cas# Qual 1 Trisiloxane, 1,1/1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 33 2 Benzoic acid, 2/4-bis[(trimethylsil 370 C16H30048i3 010586-16-0 32 3 N-Methyladrepéline, tri-TMS 413 C19H39NO3Si3 000000-00-0 25 4 Cyclopentasfloxane, decamethyl- __370 C10H3005Si5 __000541-02-6 17 ‘Abundance rp “Scan 2585 (28.487 min): LBD ©) m/z 73.00 100.008 5000: 147 | aah 281 385 | " " 4 28.20 28.40 28.60 _28.80 45 447 sgt 289 ag7 401429, w]e 147-00 34-30 miz>___..40_ 60_ 80_ 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420. | Abundance: #52459: A aerane, 1,4,1,5,5,5-hexamethyl-3,3-bis[(trimet | | | 7 } 281 5000 | . (28.20 28.40 28.60 28.80 | 369 m/z 221.0, 18.36% . | 207 249 a 1 rmiz-->___"“40 60. 80.100 420 140 160 180 200 250 240 260 280 300 320 340 360 360 400.420 | | oundance : | | 73 ' ~| 28.20 28.40 28.60 28.80 5000: 355 m/z 355.0 16.77 45 i 133 193 223 281 miz-> "0. 60. 80 100120 140 160 180 200 220 240 280 280 300 320 340 360 380 400 420 Abundance #54808: N-Methyiadrenaline, tr-TMS 28.20 28.40 28.60 28.80 i m/z 281.00 15.10% fas 355 | | | | 45 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400.420 2820 2840 2860 2880. | LB.D GCMS0103.M Wed Jan 09 12:33:50 2002 Page 9 NYC-WTC_000017358

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NYC-WTC_000017358Source: NYC Law Department, mirrored locally

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