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GCMS analysis log for sample AD31020

Machine-extracted title · confidence 95%

Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31020 on January 18, 2002.

NYC-WTC_000017459–000017477

Folder label: “GCMS X 12/20/01 A 1/8/02”

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NYC 9/11 Public Portal Document a . Library Search Compound Report ‘Data File : C:\HPCHEM\1\DATA\JAN0802\31020.D Vial: 15 , Acq On : 9 Jan 2002 2:59 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L TESS ISS IIIS E ISS ISI ISIE IESE SCI ICO SISS IOC SSIO IGE IIS IIE Peak Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 5 R.T. EstCone Area Relative to ISTD R.T. 11.00 2.28 ug/1 534963 1,4-Dichlorobenzene-d4 11.52 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H2404si4 000556-67-2 86 2 2-Oxo-4-phenyl-6~ (4-chlorophenyl)-1 282 C16H11C1N20 000000-00-0 9 3 6,7-Benzo-phenothiazine-5,5-dioxide 281 C1é6H11NO2S 000000-00-0 9 4 Benzene, 1-phenyl-4-(2-cyano-2-phen 281 C21H15N ————(027869-56-3 9 Abundance ~~~" Sean 646 (10.990 min): 31020.D ¢)” 28 [Pe 281.0; 100.00! 1 | I 73 133 493) 249 265 10.60 10.80 11.00. 14.20. 11.40 177 207 6010.80.11. u BEE 8 IE te SS IT lle PP aS m/z 282.00 28.60 miz>___40 60 80 100 120 140 160 180 _200 220 240 260. 280. ‘Abundance #41966: Cyclotetrasiloxane, octamethyl- 21 5000. | * 10.60 10.80 11.00 11.20 11.40 | [m/z 283.00 17.71 73 183 4eg.177 191 707 pag 249 205 || | imz-> 4060-80100 120 140 160 180 200 220 240 260 280 | | Abundance eR Oi ny wp tk | sr | | 10/60 10160 11:00 11.20 11.40 5000. m/z 192.90 13.02% 102123 140 475 204 247 | | mmiz-> ___40__60__ 80 100 120 140 160 180 _200 220 240 260 280 | ‘Abundance #39602: 6,7-Benzo-phenothiazine-5 ,5-dioxide | 1 | 10160 10:80 11100 19.20 11.40 | m/z 133.00 10.86% sso | 102 118 189 a | 22 iz—> 40 60 80 100 120 140 160 180 200 220 240 260 280 | 10.60 10.80 11.00 11.20 11.40 31020.D GCMS0103.M Wed Jan 09 12:11:32 2002 Page 3 NYC-WTC_000017468 :

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NYC-WTC_000017468Source: NYC Law Department, mirrored locally

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