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GCMS analysis log for sample AD31073

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

NYC-WTC_000017434–000017458

Folder label: “GCMS X 12/20/01 A 1/8/02”

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Scanned page image, NYC-WTC_000017443
OCR text

OCR status: ocr · source: ours

NYC 9/11 Public Portal Document = Library Search Compound Report © + ‘Data File : C:\HPCHEM\1\DATA\JAN0802\31073.D Vial: 10 Acq On : 8 Jan 2002 10:07 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESSIE OSS IIS OISI IIS DIOI SITIOS I SSRIS IIIS IEE IIA III Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 7 R.T. EstCone Area Relative to ISTD R.T. 11.00 2.14 ug/l 532290 1, 4-Dichlorobenzene-d4 11.53 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasilefane, octamethyl- 296 CeH2404Si4 000556-67-2 86 2 6,7-Benzo-pHenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 3 3,6-Bis (j¥“dimethylamino) -9-ethylcar 281 C18H23N3 057103-04-5 9 4 Benzene, 1-phenyl-4-(2-cyano-2-phen 281 C21H15N ____027869-56-3 9 ‘Roundance Z ‘Sean 648 (10.887 min}: $1073.0 () m/z 281.00 100.008 2ei | i | 73 a98 193 297 249 265 | t0'60 10.80 1100 11.20 11.40 | AS EO 8 08 NT 08 TT hate 221,238 m/z 282.00 28.92 miz->____40 60.80 100 120 140 160 160 200 220 240 260 260 “Abundance #72646: Cyciotetrasiloxane, octamethyl- 261 | | 000. 10.60_10.80_11.00_14.20_11.40_| ass | | M/Z 283.00 16.80 4550 78 133 477 193207 agg { mz 40 60 80 100 120 140 160 180 200 220 240 260 280 | Abundance ‘ 221 ] 4016010180. 11.00_ 11120 11:40 | 5000: m/z 192-9 12.12% | 102 118 489 204 soni | | miz->____40__ 60 _ 80100 120 140 _160__180 200 220 240 260 280 _ | | Abundance #39624: 3,6-Bis(N-dimethylamino)-9-ethyicarbazole + 2¢1 | 1060 "10.80. 11100 11.20 1140 | m/z ae 11.493) v0 elf fo | ] 44 208 222 237 250 I mz> 40 60. 80 100 120 140 160 100 200 290 240 260 260 | 10160 10.60 11100 11.20 11140 31073.D GCMS0103.M Wed Jan 09 12:19:01 2002 Page 2 NYC-WTC_000017443

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NYC-WTC_000017443Source: NYC Law Department, mirrored locally

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