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GCMS analysis log for sample AD31073

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

NYC-WTC_000017434–000017458

Folder label: “GCMS X 12/20/01 A 1/8/02”

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Scanned page image, NYC-WTC_000017442
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NYC 9/11 Public Portal Document oe Library Search Compound Report ., ¢ “Ddta File : C:\HPCHEM\1\DATA\JAN0802\31073.D Vial: 10 Acq On : 8 dan 2002 10:07 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Prereeetrerrrrrrererr ert Terre rrr rrrererrrtrrrtrrtrttt ttt ttre rt rrr irre s Peak Number 1 1,3-Dioxolane, 2-methyl- Concentration Rank 4 R.T. | EstCone Area Relative to ISTD R.T. 7.46 4.35 ug/1 1084220 1,4-Dichlorobenzene-d4 11.53 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 1,3-Dioxolgefe, 2-methyl- 88 C4Hs02 000497-26-7 9 2 Silane, pétramethyl- 88 C4H12S8i 000075-76-3 9 3 N-Ethy#formamide 73 C3H7NO 000627-45-2 9 _4 3-Pefitanol, 3-methyl- __102 C6H140 __000077-74-7 9 bundan ‘Scan 263 (7.463 miny: 31073. ¢) [m/z 73.00 100909 } 43 \ ] ar | "720-740 7.60 7.80 381,11, $0 £8,606 18-\m/z 43.00 33.17 mio __"10. 20's. 40 's0. 6070600 100.110. | | ‘Abundance “HO2002: 1,3-Dioxolane, 2-methyl- | | | i | | 5000 43 | | i | 2 | 7.20 7407.80 7.80 m/z 41.00 11.64 Fa | 3 {ns ® \ vz-> "40-0 30 87D Bw T0081. ‘Abundance Bik z | ee ; 73 ‘ 720740 7.60 7.80 5000 [m/z 44.9 11.36% H as i i 18 5359 88 Abundance Wee: NEthyormamide 5 _ 7.20 _ 740 7.60 7.80 _ fj m/z 71.00 6.70: 5000- | 44 58 16 i | | me 10 20 9% «640 «680 O10, 720 740. 7.60. 7.80. | 31073.D GCMS0103.M Wed Jan 09 12:18:57 2002 Page 1 NYC-WTC_000017442 :

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Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31024 performed on January 18, 2002.

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