GCMS analysis report for sample AD31131 showing detection of unknown compounds and surrogate recovery data from February 11, 2002.
NYC-WTC_000018972–000018982Folder label: “GCMS X 12/21/01 A 1/10/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C: \HPCHEM\ 1\DATA\JANO 802\31131.D vial: 19 ■ Acq On : 10 Jan 2002 7:22 am Operator: 209 GALOS Sample : gems scan 12/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
14.17 0.26 ug/1 91964 Naphthalene-d8 15.13
Hit# of 5 tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 59 2 Benzeneethanamine i N- (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 37 3 Benzoic acid, 2,6-bis (trimethylsil 370 C16H30O4Si3 003782-85-2 37 4 Benzoic/acid, 2,5-bis(trimethylsilo 370 Cl6H30O4Si3 003618-20-0 32 Abundance 73 Scan 994 (14.172 mln): 31131.D (-) [ m/z 73.00 100.00%
5000 267 355 45 133 154 177 193 , 223 251 । 13.80 14.00 14.20 14.40 14.60 i 1 *11r* *11 •1 “, aumnnmuun 96 —nuuwutr 323339 1 “II—u—uTm m/z 267.00 39.24% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 .... . 267 5000 13.80 14.00 14.20 14.40 14.60 m/z 355.05 30.96 191207 251 323339 1 i t । i i • i । i i i i j i -< > i । i i i < । > i i < । i i > > । i i i > ] i i i i । > > i i j i i i > । । i i i । i
■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74573 emzennethanemre, N-(pentafupropherytneafyec: 73
13.80 14.00 14.20 14.40 14.60 5000- m/z 356.0.5 10.84 267 44 151 179 209 250 |; miz-> 40 60 80 100 120 140 160 180 200 220 240 260 *280 300 320 340 360 Abundance #51296: Benzoic acid, 2,6-bis[(trimethylsilyl)oxy]-, trimet 73 355 13.80 14.00 14.20 1440 14.60 m/ z 74.00 9.51 5000
147 267 47 “ *“I n ‘ ' I • ’ ’’ I ‘ _L 208 . j d. 283 249 ‘ 1 1 * “ I ‘ I ‘ 1 1 * ‘ 1 ‘ 1 * ’ “ I 1 1 ‘ 1 1 TirTT'“ "I‘I41141 ’ 1 “ ‘11 ‘ “ I * “ 370 TTT ‘ I ' ‘ * I ‘ ‘ i-r-p-r-r-r-rr m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 13.80 14.00 14.20 14.40 14.60
31131.D GCMS0103.M Wed Feb 06 09:19:21 2002 Page 3
NYC-WTC_000018981
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NYC-WTC_000019004
GCMS analysis report for sample AD31130 showing detection of unknown compounds and surrogate recovery data from February 11, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018983
GCMS analysis report for sample AD31135 showing detection of unknown compounds and surrogate recovery data from February 11, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019025
GCMS analysis report for sample AD31217 showing detection of unknown compounds and surrogate recovery data from February 11, 2002.
Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019015
GCMS analysis report for sample AD31216 showing detection of unknown compounds and surrogate recovery data from February 11, 2002.
Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018994
Laboratory report documenting GCMS analysis of sample AD31133 performed on February 11, 2002, including detection of unknown compounds.
Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017969
Laboratory report documenting GCMS analysis of sample AD30473 conducted on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017069
Laboratory report detailing GCMS analysis of sample AD30350 including DDD surrogates on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017958
Laboratory report documenting GCMS analysis of sample AD30489 conducted on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016970
Laboratory report detailing GCMS analysis of sample AD31345 conducted on February 11, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036831
Gas chromatography-mass spectrometry analysis of sample AD29666 identifying unknown compounds and surrogate recovery data (2,4-DDD at 72%), January 28, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049851
Laboratory report showing GCMS analysis of sample AD29519 including unknown compounds and surrogate recovery data.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049723
GCMS analysis report for sample AD31632 conducted on February 11, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018934
Single-page document containing GCMS data or metadata associated with the WTC site in early January 2002.
Filed in the same folder
NYC-WTC_000018935
Page showing sample preparation parameters including drip rates and volumes for GCMS analysis from January 2002.
Filed in the same folder
NYC-WTC_000018941
GCMS calibration report for sample AD31129 listing response factors and concentrations for multiple organic compounds from January 10, 2002.
Filed in the same folder
NYC-WTC_000018945
Calibration table listing deuterated standards and retention times for GCMS analysis of sample AD31129 from January 9-10, 2002.
Filed in the same folder
NYC-WTC_000018948
GCMS reference analysis report for sample AD31129 listing component names and values from January 10, 2002.
Filed in the same folder